Unlock instant, AI-driven research and patent intelligence for your innovation.

Quartz glass and preparation method thereof

A quartz glass and compound technology, applied in glass manufacturing equipment, glass molding, manufacturing tools, etc., can solve problems such as inability to meet semiconductor application requirements, corrosion, and fast corrosion rates

Active Publication Date: 2017-02-01
CHINA BUILDING MATERIALS ACAD
View PDF3 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Si-O chemical bonds are easily corroded by hydrofluoric acid. According to calculations, in the hydrofluoric acid environment, the corrosion rate of quartz glass composed entirely of Si-O chemical bonds has reached 150 μm / h. The corrosion rate is faster in hydrofluoric acid environment, which cannot meet the application requirements of semiconductor etching in hydrofluoric acid environment

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Quartz glass and preparation method thereof
  • Quartz glass and preparation method thereof
  • Quartz glass and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0061] Such as figure 1 Shown, a kind of preparation method of quartz glass that one embodiment of the present invention proposes, it comprises:

[0062] Step 10, using a dissolving agent to dissolve and mix the first doping compound and the second doping compound to form a doping mixed solution, the first doping compound is an aluminum-containing compound, and the second doping compound includes a Zr-containing compound, At least one of Y-containing compounds, La-containing compounds, Sc-containing compounds, Th-containing compounds, V-containing compounds, and Ti-containing compounds;

[0063] Wherein, the dissolving agent can be a kind of dissolving agent, which can dissolve the first doping compound and the second doping compound simultaneously; or, the dissolving agent can include two kinds of dissolving agents, one kind of dissolving agent is used to dissolve the first Doping compound, another dissolving agent is used to dissolve the second doping compound, forming a do...

Embodiment approach

[0112] 1. Vacuum electric melting process melting method:

[0113] The crystalline doped silica powder is ground, and the doped silica powder after grinding is sieved to obtain the sieved silica powder, and the sieved The silicon dioxide powder is melted into the finished quartz glass by melting process at 1000-2500 degrees Celsius, specifically:

[0114] Sieve the doped silica powder after grinding to obtain doped silica powder with particles in the range of 20 to 200 mesh, and melt the doped silica powder with 20 to 200 mesh by vacuum electrofusion process The finished quartz glass.

[0115] 2. High-frequency plasma melting process Melting method:

[0116] The crystalline doped silica powder is ground, and the doped silica powder after grinding is sieved to obtain the sieved silica powder, and the sieved The silicon dioxide powder is melted into the finished quartz glass by melting process at 1000-2500 degrees Celsius, specifically:

[0117] Sieve the doped silica powder...

Embodiment 2

[0132] A kind of quartz glass that one embodiment of the present invention proposes, comprises:

[0133] Quartz glass finished product, prepared by the preparation method of said quartz glass finished quartz glass;

[0134] The preparation method of described quartz glass comprises:

[0135] The first doping compound and the second doping compound are dissolved and mixed by a dissolving agent to form a doping mixed solution, the first doping compound is an aluminum-containing compound, and the second doping compound includes a Zr-containing compound and a Y-containing compound , at least one of La-containing compounds, Sc-containing compounds, Th-containing compounds, V-containing compounds, and Ti-containing compounds;

[0136] Parts by volume L 1 silicon alkoxide, parts by volume L 2 of water, parts by volume L 3 Alcoholic organic solvents are mixed to form a silicon alkoxide solution;

[0137] The silicon alkoxide solution, the doping mixed solution and the catalyst ar...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to quartz glass and a preparation method thereof, relates to the technical field of quartz glass manufacture, and mainly aims to improve corrosion resistance of quartz glass finished products under the environments containing fluorine such as hydrofluoric acid and fluorine gas F2. The method includes the steps: dissolving and mixing first doping compounds and second doping compounds by the aid of dissolving agents to form doping mixed solution; performing hydrolysis condensation reaction for silanol saline solution, the doping mixed solution and catalyst to obtain doping silica gel; firing the doping silica gel to prepare the quartz glass finished products. The first doping compounds are compounds containing aluminum, quartz glass finished products contain Al2O3 and at least one in ZrO2, Y2O3, La2O3, Sc2O3, ThO2, V2O5 and TiO2, and the doping mixed solution is fired into the Al2O3, the ZrO2, the Y2O3, the La2O3, the Sc2O3, the ThO2, the V2O5 and the TiO2. Holes in a tetrahedron network structure of SiO2 are filled with the Al2O3, the ZrO2, the Y2O3, the La2O3, the Sc2O3, the ThO2, the V2O5 and the TiO2 by the aid of a network middle body or a network outside body, and the quartz glass is resistant in acid corrosion.

Description

technical field [0001] The invention relates to the technical field of quartz glass manufacturing, in particular to a method for preparing quartz glass and the quartz glass. Background technique [0002] Quartz glass is an amorphous material with silicon dioxide as the main component. Its microstructure is a simple network composed of silicon dioxide tetrahedral structural units. Because the Si-O chemical bond energy is large and the structure is very tight, so Quartz glass has unique properties, such as high temperature resistance, low expansion coefficient, thermal shock resistance, high chemical stability and good electrical insulation properties. [0003] Due to the unique properties of quartz glass, it is an irreplaceable ideal auxiliary material in the manufacturing process of semiconductor integrated circuits, including quartz glass tubes, quartz glass sheets, quartz glass rings, quartz glass plates, quartz glass flanges, quartz glass groove boats, Quartz glass clean...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C03C3/06C03C1/02C03C6/08C03B20/00
CPCC03B19/066C03C1/026C03C3/06C03C2201/36
Inventor 聂兰舰向在奎贾亚男王蕾邵竹锋王慧张辰阳符博王玉芬
Owner CHINA BUILDING MATERIALS ACAD