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Axial micro-catalytic reaction unit and application thereof

A catalytic reaction and micro-reaction channel technology, applied in chemical instruments and methods, chemical/physical processes, chemical/physical/physicochemical processes, etc., can solve problems such as short residence time, local overheating, and large height and diameter, and achieve Guaranteed smooth operation, extended service life, and reduced production costs

Active Publication Date: 2017-02-08
SINOPEC ENG +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Axial reactor design, relatively easy processing, and simple operation, but there are problems with large reactor equipment, large bed pressure drop, prone to local overheating, slow heat transfer, low conversion rate, obvious amplification effect, and the need for materials for the reactor. higher grade questions
The radial bed reactor has a large height-to-diameter ratio, a small bed pressure drop, and a short residence time of the reactants in the catalyst bed, but it is difficult to achieve uniform distribution of the reactants in the radial direction, and the production intensity of the unit catalyst bed is low
[0003] In order to overcome the problems of low heat transfer and mass transfer efficiency in traditional chemical industry, microchemical technology emerged in the 1980s and 1990s.

Method used

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  • Axial micro-catalytic reaction unit and application thereof
  • Axial micro-catalytic reaction unit and application thereof
  • Axial micro-catalytic reaction unit and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0051] Such as figure 1 As shown, the axial micro-catalytic reaction unit adopted in this embodiment includes a cylindrical column 1 composed of a top sealing plate, a bottom sealing plate and side surfaces. The up and down of the column body 1 are in fluid communication through the micro-reaction channel 2 . Such as Figure 9 As shown, in the micro-reaction channel 2 of the conical tube structure, the tube wall is coated with nickel, an active component of methanation reaction, and the two ends are respectively sealed and connected with the top sealing plate and the bottom sealing plate of the column body 1 .

[0052] The height of the axial micro-catalytic reaction unit is 100 mm, and the diameter is 340 mm. The length of the micro-reaction channel of the tapered tube is 100 mm, the diameter of the inlet of the tapered tube is 10 mm, and the diameter of the outlet is 4 mm. The proportion of the column volume is 41.6%.

[0053] The axial micro-catalytic reaction unit can b...

Embodiment 2

[0055] Such as figure 2 As shown, the difference between embodiment 2 and embodiment 1 is that the diameter of the tapered pipe inlet is 4mm, and the diameter of the outlet is 10mm. This type of reactor is suitable for chemical reactions with increased reaction volume, such as cyclohexane dehydrogenation, ethylbenzene dehydrogenation Hydrogen and ammonia decomposition reactions.

[0056] The axial micro-catalytic reaction unit is used for cyclohexane dehydrogenation reaction. The dehydrogenation reaction of cyclohexane is an endothermic reaction with volume increase. Cyclohexane enters the conical tube whose inner surface is coated with platinum metal from above the axial micro-catalytic reaction unit, and the dehydrogenation reaction occurs on the surface of the platinum metal catalyst, from The product outlet exits the conical tube. Cyclohexane flows from the inside to the outside, and the reaction channel gradually becomes larger, which increases the driving force for th...

Embodiment 3

[0058] Such as Figure 6 and Figure 7 As shown, the difference between embodiment 3 and embodiment 1 is that three axial micro-catalytic reaction units arranged side by side composed of quadrangular column 1 are used for the methanation reaction together, and the top of the axial micro-catalytic reaction unit Both the sealing plate and the bottom sealing plate are hermetically connected.

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Abstract

The invention discloses an axial micro-catalytic reaction unit and application thereof. The axial micro-catalytic reaction unit is characterized in that the axial micro-catalytic reaction unit comprises a column and micro-reaction channels axially penetrating the column; the place above the column is communicated with a fluid below the column only through the micro-reaction channels; and the the micro-reaction channels are provided with upper micro-reaction channel openings and lower micro-reaction channel openings with different diameters. The axial micro-catalytic reaction unit provided by the invention can be applied to reactions with changes in reaction volume, enables the usage amount of a catalyst to be small, and is low in pressure drop, short in retention time, high in space utilization rate and free of the phenomena of bias current and short circuit of gas.

Description

technical field [0001] The invention relates to an axial micro-catalysis reaction unit and its application. Background technique [0002] At present, there are mainly two types of fixed bed reactors, one is axial fixed bed reactor, and the other is radial fixed bed reactor. Axial reactor design, relatively easy processing, and simple operation, but there are problems with large reactor equipment, large bed pressure drop, prone to local overheating, slow heat transfer, low conversion rate, obvious amplification effect, and the need for materials for the reactor. high-level issues. The radial bed reactor has a large height-to-diameter ratio, a small bed pressure drop, and a short residence time of the reactants in the catalyst bed, but it is difficult to achieve uniform distribution of the reactants in the radial direction, and the production intensity of the unit catalyst bed is low. [0003] In order to overcome the problems of low heat transfer and mass transfer efficienc...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/00
Inventor 张旭戴文松王子宗蒋荣兴
Owner SINOPEC ENG
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