Unlock instant, AI-driven research and patent intelligence for your innovation.

Identification method for parched white peony root in Shiquan Dabu wine

A technology of Shiquan Dabu wine and fried white peony, which is applied in the field of traditional Chinese medicine detection to achieve good reproducibility, ensure product quality, and scientifically and effectively identify the effect

Inactive Publication Date: 2017-02-22
GUIZHOU XINBANG PHARMACEUTICAL CO LTD
View PDF7 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the existing quality standards of Shiquan Dabu wine, the identification of fried Radix Paeoniae Alba is not involved. Therefore, to study a method that is easy to operate and can efficiently and quickly identify the fried Radix Paeoniae Alba in Shiquan Dabu wine will help improve the quality of Shiquan Dabu wine. The quality inspection standard of Quanda tonic wine is particularly necessary

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Identification method for parched white peony root in Shiquan Dabu wine
  • Identification method for parched white peony root in Shiquan Dabu wine
  • Identification method for parched white peony root in Shiquan Dabu wine

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] The identification method of fried white peony in Shiquan Dabu wine includes the following steps:

[0044] (1) Preparation of the test solution: Take 25 mL of this product, add 25 mL of n-butanol and shake to extract, obtain n-butanol liquid, evaporate to dryness, add 2 mL of methanol to the residue to dissolve it, and use it as the test solution;

[0045] (2) Preparation of reference substance solution: take paeoniflorin reference substance, add methanol to make a solution containing 1 mg of paeoniflorin reference substance per 1 mL, as the reference substance solution;

[0046] (3) Identification: According to the "Chinese Pharmacopoeia" 2015 edition four general rules 0502 thin-layer chromatography test, absorb 9 μL of the reference substance solution and 9 μL of the test solution, respectively spot on the same silica gel G thin-layer plate, with chloroform-acetic acid Ethyl ester-methanol-formic acid=35︰3︰8︰0.1 is the developer, develop, take out, dry, spray with 5%...

Embodiment 2

[0048] The identification method of fried white peony in Shiquan Dabu wine includes the following steps:

[0049] (1) Preparation of the test solution: Take 35 mL of this product, add 45 mL of n-butanol and shake to extract, obtain n-butanol liquid, evaporate to dryness, add 3 mL of methanol to the residue to dissolve it, and use it as the test solution;

[0050] (2) Preparation of reference substance solution: take paeoniflorin reference substance, add methanol to make a solution containing 1 mg of paeoniflorin reference substance per 1 mL, as the reference substance solution;

[0051] (3) Identification: According to the "Chinese Pharmacopoeia" 2015 edition four general rules 0502 thin-layer chromatography test, absorb 12 μL of the reference substance solution and 12 μL of the test solution, respectively spot on the same silica gel G thin-layer plate, with chloroform-acetic acid Ethyl ester-methanol-formic acid=45:8:15:0.3 is the developer, develop, take out, dry, spray with...

Embodiment 3

[0053] The identification method of fried white peony in Shiquan Dabu wine includes the following steps:

[0054] (1) Preparation of the test solution: take 20mL of this product, add 30mL of n-butanol and shake to extract to obtain n-butanol liquid, evaporate to dryness, add 1mL of methanol to the residue to dissolve it, and use it as the test solution;

[0055] (2) Preparation of reference substance solution: take paeoniflorin reference substance, add methanol to make a solution containing 1 mg of paeoniflorin reference substance per 1 mL, as the reference substance solution;

[0056] (3) Identification: According to the "Chinese Pharmacopoeia" 2015 edition four general rules 0502 thin-layer chromatography test, absorb 10 μL of the reference substance solution and 10 μL of the test solution, respectively spot on the same silica gel G thin-layer plate, and use chloroform-acetic acid Ethyl ester-methanol-formic acid=40:5:10:0.2 is the developer, develop, take out, dry, spray wi...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses an identification method for parched white peony root in Shiquan Dabu wine, and particularly relates to a thin-layer chromatography method with a paeoniflorin reference substance as a control and with a mixture with chloroform:ethyl acetate:methanol:formic acid=(35-45):(3-8):(8-15):(0.1-0.3) as a developer. The identification method for the parched white peony root in the Shiquan Dabu wine can efficiently and accurately identify the parched white peony root component in the Shiquan Dabu wine. The method is simple and easy to operate, strong in controllability and specificity, high in degree of separation, high in sensitivity and good in reproducibility, a negative control has no interference, and different manufacturers of thin-layer plates and temperature and humidity conditions do not affect the method. The identification method can accurately, comprehensively, scientifically and effectively identify the parched white peony root component in the bone pain medicated wine, improves quality detection standards, and further ensures the stability, safety and effectivity of the product quality,.

Description

technical field [0001] The invention relates to a method for identifying fried Radix Paeoniae Alba in Shiquan Dabu wine, and specifically belongs to the technical field of traditional Chinese medicine detection. Background technique [0002] Shiquan Dabu wine is made from Codonopsis pilosula, Atractylodes macrocephala (stir-fried), Poria cocos, licorice (honey-roasted), angelica, Chuanxiong, white peony (stir-fried), rehmannia glutinosa, astragalus (honey-roasted) and cinnamon. The auxiliary materials are liquor and sucrose. The function of this product is to warm and invigorate qi and blood. Rehmannia glutinosa nourishes blood and nourishes yin, replenishes essence and produces marrow; Codonopsis pilosula nourishes spleen and invigorates the middle, nourishes qi and produces blood, yang produces yin and grows, and it is a king medicine. Atractylodes invigorates the spleen and qi; Poria cocos invigorates the spleen and dampness; Astragalus invigorates the spleen and invigo...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90
CPCG01N30/90
Inventor 罗治桃
Owner GUIZHOU XINBANG PHARMACEUTICAL CO LTD