Washing method of crude adipic acid slurry in adipic acid production process
A production process and washing method technology, applied in the separation/purification of carboxylic acid compounds, organic chemistry, etc., can solve problems such as viscosity drop, unsatisfactory, and high end-breakage rate, and achieve reduced nitrate content, reduced emissions, Realize the effect of green production
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Embodiment 1
[0036] use figure 1 The process flow for the washing of the crude adipic acid slurry from the crude acid crystallization process.
[0037] (1) Send the crude adipic acid slurry from the crude acid crystallization process into the crude adipic acid thickener 1 to obtain thickened adipic acid slurry with a weight solid content of 35%;
[0038] In described thick adipic acid slurry, contain the component of following percentage by weight:
[0039] Adipic acid 34%, nitrate balance 19%, dibasic acid 8%, water 37%.
[0040] (2) Then the thickened adipic acid slurry obtained is sent into the crude acid centrifuge 2, and the original process water from the original process water tank 3 is used to 3 / h flow for washing, and liquid-solid separation to obtain wet adipic acid;
[0041] The weight ratio of thickened adipic acid slurry to former process water is:
[0042] Thickened adipic acid slurry: original process water = 1:0.8;
[0043] The washing water discharged from the crude ...
Embodiment 2
[0052] use figure 1 The process flow for the washing of the crude adipic acid slurry from the crude acid crystallization process.
[0053] (1) Send the crude adipic acid slurry from the crude acid crystallization process into the crude adipic acid thickener 1 to obtain thickened adipic acid slurry with a weight solid content of 45%;
[0054]In described thick adipic acid slurry, contain the component of following percentage by weight:
[0055] Adipic acid 37%, nitrate balance 14%, dibasic acid 7%, water 40%.
[0056] (2) Then the thickened adipic acid slurry obtained is sent into the crude acid centrifuge 2, and the original process water from the original process water tank 3 is used to 3 / h flow for washing, and liquid-solid separation to obtain wet adipic acid;
[0057] The weight ratio of thickened adipic acid slurry to former process water is:
[0058] Thickened adipic acid slurry: original process water = 1:1.2;
[0059] The washing water discharged from the crude a...
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