Supported alloy type hydrogenation saturated catalyst and preparation method thereof
A catalyst and alloy-type technology, which is applied in the field of loaded alloy-type hydrogenation saturation catalyst and its preparation, can solve the problems of poor stability and low hydrogenation saturation selectivity, and achieve the effect of good stability and strong saturation capacity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0031] Add 2.4g of scallop powder to 80g of γ-alumina (commercially purchased) on a dry basis and mix well, then add 4g of HNO at a volume ratio of 1:1 3 aqueous solution and 40g deionized water, and knead evenly to make a dough suitable for extrusion. It is extruded through a die and is in the shape of a slender cylinder (cross-sectional diameter 1.5mm). After drying at 120°C, it is baked at 550°C for 4 hours, and then it is cut into carrier particles (1.5×4.0mm) of uniform size for use.
[0032] A mixed solution of palladium nitrate, cobalt nitrate, and tin chloride was used to impregnate the carrier particles at 40°C. The dry basis weight of the carrier contained in the impregnation solution was 0.2%Pd, 3%Co and 0.5%Sn, aged for 8h and passed After drying, it was oxidized in air at 900°C for 4 hours, and then reduced in hydrogen at 700°C for 4 hours (this step can be completed in a reactor) to obtain the finished catalyst 1.
[0033] Catalyst 1 was used to evaluate the hyd...
Embodiment 2
[0035] Add 2.4g of kale powder to 80g of silica (commercially purchased) on a dry basis and mix well, then add 4g of HNO with a volume ratio of 1:1 3 aqueous solution and 40g deionized water, and knead evenly to make a dough suitable for extrusion. It is extruded through a die and is in the shape of a slender cylinder (cross-sectional diameter 1.5mm). After drying at 120°C, it is baked at 550°C for 4 hours, and then it is cut into carrier particles (1.5×4.0mm) of uniform size for use.
[0036] A mixed solution of palladium nitrate, cobalt nitrate, and tin chloride was used to impregnate the carrier particles at 40°C. The dry basis weight of the carrier contained in the impregnation solution was 0.2%Pd, 3%Co and 0.5%Sn, aged for 8h and passed After drying, oxidize in air at 900°C for 4 hours, and then reduce in hydrogen at 700°C for 4 hours (this step can be completed in a reactor) to obtain the finished catalyst 2.
[0037] Catalyst 2 was used to evaluate the hydrogenation sa...
Embodiment 3
[0039] Add 2.4g of scallop powder to 80g of titanium oxide (commercially purchased) on a dry basis and mix well, then add 4g of HNO at a volume ratio of 1:13 aqueous solution and 40g deionized water, and knead evenly to make a dough suitable for extrusion. It is extruded through a die and is in the shape of a slender cylinder (cross-sectional diameter 1.5mm). After drying at 120°C, it is baked at 550°C for 4 hours, and then it is cut into carrier particles (1.5×4.0mm) of uniform size for use.
[0040] A mixed solution of palladium nitrate, cobalt nitrate, and tin chloride was used to impregnate the carrier particles at 40°C. The dry basis weight of the carrier contained in the impregnation solution was 0.2%Pd, 3%Co and 0.5%Sn, aged for 8h and passed After drying, oxidize in air at 900°C for 4 hours, and then reduce in hydrogen at 700°C for 4 hours (this step can be completed in a reactor) to obtain the finished catalyst 3.
[0041] Catalyst 3 was used to evaluate the hydrogena...
PUM
| Property | Measurement | Unit |
|---|---|---|
| boiling point | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More