Crystallization method of thiamine mononitrate
A technology of thiamine nitrate and thiamine sulfate, applied in the direction of organic chemistry, can solve the problems of poor crystal fluidity, small bulk density, and low market competitiveness
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[0024] The first step of mixing: take 380kg (pure amount) of thiothiamine, a synthetic intermediate of vitamin B1, and obtain about 3500kg of thiamine sulfate solution through oxidation in a temporary storage tank, put 90kg of ammonium nitrate into a heating tank containing 80kg of purified water In the pot, heat the temperature above 50°C to completely dissolve the ammonium nitrate, then lower the temperature properly, add the ammonium nitrate solution to the thiamine sulfate solution in the temporary storage tank and mix well, and the mixing temperature is controlled at 20-25°C. After the mixing is completed, keep the temperature of the above mixed solution at 20-25°C and store it in a turnover container for future use.
[0025] The second part of mixing: Add 100kg of purified water with a temperature of 20-25°C into the refining reactor to ensure that the stirring of the refining tank can touch and stir the purified water, turn on the stirring, and control the speed at 20r / m...
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