Aluminum titanium boron carbon zirconium rare earth refiner, preparation method and application thereof
A technology of aluminum titanium boron carbon and refiner, which is applied in the field of alloys, can solve the problems of long refinement time, short timeliness, uneven structure of aluminum master alloy grain refiner, etc., and achieve the effect of excellent performance
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Embodiment 1
[0032] The manufacture method of aluminum titanium boron carbon zirconium rare earth grain refiner (Al-Ti5-B0.2-C0.1-Zr0.1-Re1) comprises the following steps connected in sequence:
[0033] 1) Mix potassium fluotitanate, potassium fluoborate, potassium fluozirconate, and graphite recarburizer at a speed of 50 rpm for 15 minutes;
[0034] 2) melting the aluminum ingot;
[0035] 3) After the aluminum ingot is completely melted, add the material obtained in step 1) into the molten aluminum for a reaction at a temperature of 800°C, and the reaction time is 25 minutes;
[0036] 4) After the reaction finishes, scoop off the slag;
[0037] 5) Add a solvent of 2% of the mass of the aluminum ingot for stirring and degassing refining, blow the solvent into the alloy liquid with argon to carry out refining and degassing, the refining time is 22 minutes, the argon pressure is 0.2Mpa, the stirring speed is 350rpm, and the stirring time is 22 minutes. The temperature is 820°C, and the sol...
Embodiment 2
[0045] The manufacturing method of the aluminum titanium boron carbon zirconium rare earth grain refiner comprises the following steps connected in sequence:
[0046] 1) Potassium fluotitanate, potassium fluoborate, potassium fluozirconate, and graphite recarburizer were mixed at a speed of 55 rpm for 20 minutes;
[0047] 2) melting the aluminum ingot;
[0048] 3) After the aluminum ingot is completely melted, add the material obtained in step 1) into the molten aluminum for a reaction at a temperature of 850°C, and the reaction time is 30 minutes;
[0049] 4) After the reaction finishes, scoop off the slag;
[0050] 5) Add a solvent of 2% of the mass of the aluminum ingot for stirring and degassing refining, blow the solvent into the alloy liquid with argon to carry out refining and degassing, the refining time is 25 minutes, the argon pressure is 0.3Mpa, the stirring speed is 400rpm, and the stirring time is 25 minutes. The temperature is 850°C, and the solvent is a mixtur...
Embodiment 3
[0058] The manufacturing method of the aluminum titanium boron carbon zirconium rare earth grain refiner comprises the following steps connected in sequence:
[0059] 1) Mix potassium fluotitanate, potassium fluoborate, potassium fluozirconate, and graphite recarburizer at a speed of 50 rpm for 10 minutes;
[0060] 2) melting the aluminum ingot;
[0061] 3) After the aluminum ingot is completely melted, add the material obtained in step 1) into the molten aluminum for a reaction at a temperature of 750°C, and the reaction time is 20 minutes;
[0062] 4) After the reaction finishes, scoop off the slag;
[0063] 5) Add a solvent of 2% of the mass of the aluminum ingot for stirring and degassing refining, blow the solvent into the alloy liquid with argon to carry out refining and degassing, the refining time is 20 minutes, the argon pressure is 0.1Mpa, the stirring speed is 300rpm, and the stirring time is 20 minutes. The temperature is 800°C, and the solvent is a mixture of po...
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