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Filtering device and application thereof

A filter device and filter membrane technology, applied in measurement devices, instruments, scientific instruments, etc., can solve the problems of low concentration, reduced stability, and environmental pollution of solutions containing the substance to be tested.

Pending Publication Date: 2017-08-04
新疆农业科学院农业质量标准与检测技术研究所
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Traditional sample purification methods, such as liquid-liquid extraction, often take a lot of time due to the need for repeated operations, and at the same time need to use a large amount of organic solvents, such as formaldehyde, acetone, ethanol, etc., causing environmental pollution, and the separated The solution containing the substance to be tested is low in concentration and requires further purification
It can be seen that the traditional separation process takes a long time and is cumbersome. The substance to be tested is prone to changes such as decomposition and degradation during the separation process, and the stability is reduced, which affects the reliability of the test results.

Method used

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  • Filtering device and application thereof

Examples

Experimental program
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Effect test

Embodiment

[0046]Application of the filtering device of the invention to the detection of plasticizer content in edible fungi. The filtering device described in this embodiment is as figure 1 shown.

[0047] Sample extraction: Weigh 20 grams of sample into a 100 ml centrifuge tube, add 7 grams of sodium chloride, then add 40 ml of acetonitrile solution, centrifuge at 10,000 rpm for 1 minute, then absorb 10 ml of the acetonitrile extract from the upper layer, concentrate n-hexane to volume to 2.5 ml to obtain the first solution.

[0048] Sample separation: the above-mentioned first solution is passed through the filter device described in the present invention, and the filter device described in this embodiment is as follows: figure 1 shown. Filtration method is that the second rolling head 21 of the upper membrane cover 2 of the present invention is connected with the first rolling head 11 of the sample liquid chamber 1, and the third rolling head 4 of the lower membrane cover 4 of th...

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Abstract

The invention discloses a filtering device and application thereof. The filtering device comprises a sample liquid cavity and a filtering head, wherein the filtering head comprises an upper membrane cover, a filtering membrane and a lower membrane cover; the upper end of the sample liquid cavity is opened; a cavity of a first rolling head is formed in the lower end of the sample liquid cavity; a second rolling head is arranged at the upper end of the upper membrane cover; the second rolling head is embedded with the first rolling head; a third rolling head is arranged at the lower end of the lower membrane cover; the surfaces of the sample liquid cavity, the upper membrane cover and / or the lower membrane cover are made of metals. The filtering device disclosed by the invention is used for detecting a plasticizer in a sample. The invention provides the filtering device made of a metal material, the filtering device is stable in material and not liable to cause interference upon a tested sample, and the reliability of detection results is improved.

Description

technical field [0001] The invention relates to a separating device, in particular to a filtering device and its application. Background technique [0002] When samples (such as vegetables, fruits, etc.) are tested for pesticide residue analysis, a series of pretreatment processes are required, and the pretreatment process mainly includes extraction and separation. Extraction is the operation step of separating the substance to be tested from the sample, and different extraction methods can be selected according to the properties of the substance to be tested. Separation is to purify the complex components extracted from the sample and remove impurities in order to obtain accurate test results. [0003] Adsorption column chromatography is one of the traditional purification methods, and the adsorption columns are generally florisil, alumina and activated carbon columns. Traditional sample purification methods, such as liquid-liquid extraction, often take a lot of time due ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/14
CPCG01N30/14G01N2030/146
Inventor 范盈盈刘河疆康露王成赵多勇房世杰
Owner 新疆农业科学院农业质量标准与检测技术研究所