Method for preparing ferro-titanium alloy based on thermite self-propagating gradient reduction and slag washing refining
A self-propagating technology for ferro-titanium alloys, which is applied in the field of ferro-titanium alloys based on thermite self-propagating gradient reduction and slag washing refining, can solve the problems of low titanium recovery rate and incomplete reduction, and reduce aluminum residues and energy consumption , Strengthen the effect of gold slag separation process
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Embodiment 1
[0029] A method for preparing ferro-titanium alloy based on thermite self-propagating gradient reduction and slag washing refining, comprising the following steps:
[0030] (1) Thermite self-propagating gradient reduction
[0031] According to rutile, Fe 2 o 3 The mass ratio of powder, aluminum powder, and slagging agent CaO is 1.0:1.46:0.92:0.19, and their particle sizes respectively satisfy: rutile≤3mm; Fe 2 o 3Powder ≤ 0.2mm; aluminum powder particle size ≤ 2mm; slagging agent particle size ≤ 0.2mm; divide the material into 5 batches, and the amount of aluminum in each batch is 1.20, 1.05, 1.0, 0.90 of the theoretical stoichiometric ratio of thermite self-propagating reaction , 0.85 times, and the total aluminum content of raw materials is 0.96 times of the theoretical chemical dosage ratio of thermite self-propagating reaction, and the weight of the first batch of materials accounts for 20% of the total amount of materials; The powder is ignited from the top of the mat...
Embodiment 2
[0037] A method for preparing ferro-titanium alloy based on thermite self-propagating gradient reduction and slag washing refining, comprising the following steps:
[0038] (1) Thermite self-propagating gradient reduction
[0039] According to rutile, Fe 2 o 3 The mass ratio of powder, aluminum powder, and slagging agent CaO is 1.0:1.6:0.98:0.23, and their particle sizes respectively satisfy: rutile≤3mm; Fe 2 o 3 Powder ≤ 0.2mm; aluminum powder particle size ≤ 2mm; slagging agent particle size ≤ 0.2mm; divide the material into 6 batches, and the amount of aluminum in each batch is 1.20, 1.1, 0.95, 0.90 of the theoretical stoichiometric ratio of thermite self-propagating reaction . Use magnesium powder to ignite from the top of the material to initiate a self-propagating reaction, and then add other batches of materials one after another until the reaction is complete to obtain a high-temperature melt;
[0040] (2) Insulate and melt the high-temperature melt through electr...
Embodiment 3
[0045] A method for preparing ferro-titanium alloy based on thermite self-propagating gradient reduction and slag washing refining, comprising the following steps:
[0046] (1) Thermite self-propagating gradient reduction
[0047] According to rutile, Fe 2 o 3 The mass ratio of powder, aluminum powder, and slagging agent CaO is 1.0:1.72:1.04:0.38, and their particle sizes respectively satisfy: rutile≤3mm; Fe 2 o 3 Powder ≤ 0.2mm; aluminum powder particle size 2mm; slagging agent particle size ≤ 0.2mm; divide the material into 7 batches, and the amount of aluminum in each batch is 1.20, 1.1, 1.0, 0.95, 1.20, 1.1, 1.0, 0.95, 0.925, 0.90, 0.875, 0.85 times, and the total aluminum content of raw materials is 0.95 times of the theoretical chemical dosage ratio of thermite self-propagating reaction, and the weight of the first batch of materials accounts for 22.2% of the total amount of materials; put the first batch of materials into the reaction In the furnace, magnesium powde...
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