Graphene and ferroferric oxide @gold composite, and preparation method and application of graphene and ferroferric oxide @gold composite
A technology of ferric tetroxide and composite materials, applied in the field of materials, can solve problems such as unstable connection system, and achieve the effects of simple and reliable preparation method, high efficiency and mild reaction conditions
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[0033] Example 1
[0034] This embodiment provides a method for preparing graphene and ferroferric oxide@gold composite material, which includes the following steps:
[0035] (1) Construction of azide mercaptan-modified ferroferric oxide@gold complex and alkynylated graphene oxide:
[0036] Among them, the ferroferric oxide@gold complex modified with thiol azide includes the following construction steps:
[0037] A. Preparation of colloidal solution of nanometer ferroferric oxide by co-precipitation method
[0038] 2.703g FeCl 3 ·6H 2 Put O in a four-necked reaction flask system, add 100mL of three-distilled water to dissolve it, pass nitrogen protection, add 0.998g of FeCl under stirring conditions 2 ·4H 2 O, add ammonia water dropwise from the injection port to the reaction system to increase the pH of the solution to 9.2, stop adding ammonia water, continue the reaction for 15 minutes, and then heat the reaction system to 85°C for 25 minutes to obtain nano ferroferric oxide The coll...
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