Preparation method of zero shrinkage LTCC multi-layer ceramic substrate
A technology of multilayer ceramics and porous ceramics, which is applied in the preparation of zero-shrinkage LTCC multilayer ceramic substrates in the plane X\Y direction, and in the field of preparation of zero-shrinkage LTCC multilayer ceramic substrates, which can solve the difficulty of consistency control and shrinkage control. Poor precision, high material cost and other problems, to achieve the effect of loose material and equipment performance requirements, solve thermal uniformity, and simple preparation process
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[0032] Example 1:
[0033] A method for preparing the zero-shrinkage LTCC multilayer ceramic substrate of the present invention, such as figure 1 As shown, including the following steps:
[0034] (1) Prepare dupont 951 LTCC green tiles, and carry out the pre-process operations of punching, printing and positioning.
[0035] (2) Cut the LTCC green ceramic sheet 5 obtained by the previous process operation into 70mm×70mm small pieces, laminate the small pieces into 10 layers in turn, and then place two 0.1mm thick AlN ceramic green ceramic sheets on the upper and lower sides of the laminate. Put a layer on it and heat-press it at a temperature of 80°C and a pressure of 15MPa for 2 hours to form a green porcelain body.
[0036] (3) First place a porous ceramic pressing plate 3 isolation layer on the upper and lower surfaces of the green porcelain body, and then place a porous silicon carbide pressing plate 2 on the upper and lower surfaces of the porous ceramic pressing plate 3 holding t...
Example Embodiment
[0041] Example 2:
[0042] A method for preparing the zero-shrinkage LTCC multilayer ceramic substrate of the present invention, such as figure 1 As shown, including the following steps:
[0043] (1) Prepare Ferro A6 LTCC green ceramic sheet, and carry out the pre-process work of punching, printing and positioning.
[0044] (2) Cut the green ceramic slices obtained in step (1) into 70mm×70mm small slices, stack them in 20 layers in sequence, and then place two 0.1mm thick AlN ceramic green ceramic slices on top of the stack. The temperature is 90°C and the pressure is 20MPa for 1 hour to form a green porcelain embryo.
[0045] (3) First place a porous ceramic pressing plate 3 on the upper and lower surfaces of the green porcelain body, and then place a porous silicon carbide pressing plate 2 on the upper and lower surfaces of the porous ceramic pressing plate 3 holding the green porcelain body, and place it under pressure. On the device.
[0046] (4) Start the temperature rise, and in...
Example Embodiment
[0050] Example 3:
[0051] A method for preparing the zero shrinkage LTCC multilayer ceramic substrate of the present invention includes the following steps:
[0052] (1) Prepare dupont 951 LTCC green tiles, and carry out the pre-process work of punching, printing and positioning.
[0053] (2) Cut the green ceramic sheet obtained in step (1) into 70mm×70mm small pieces, and use 10 layers to sequentially stack them, and then two pieces of 0.1mm thick Al 2 O 3 Put a layer of green ceramic slices on top and bottom of the laminate, and heat-press at a temperature of 100°C and a pressure of 15 MPa for 1 hour to form a green ceramic body.
[0054] (3) First place a porous ceramic pressing plate 3 on the upper and lower surfaces of the green porcelain body, and then place a porous silicon carbide pressing plate 2 on the upper and lower surfaces of the porous ceramic pressing plate 3 holding the green porcelain body, and place it under pressure. On the device.
[0055] (4) Start the temperatur...
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