A kind of high-temperature solid foaming agent and preparation method thereof
A technology of high-temperature solids and foam discharge agent, applied in chemical instruments and methods, drilling composition and other directions, can solve the problems of unsuitable gas wells, inconvenient storage and filling, and poor drainage effect.
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[0021] Specific embodiments: the present invention will be further described below in conjunction with embodiment: a kind of high-temperature solid foaming agent, it is made of alkyl sulfate, lauryl ammonium sulfate C 12 h 25 SO 4 NH 4 , stearic acid C 18 h 36 o 2 , sodium carbonate Na 2 CO 3 And water composition, their weight percentage is: alkyl sulfate 20% ~ 30%, lauryl ammonium sulfate C 12 h 25 SO 4 NH 4 10%~15%, stearic acid C 18 h 36 o 2 25%~35%, sodium carbonate Na 2 CO 3 8%~12%, the rest is water;
[0022] A kind of preparation method of high temperature solid foaming agent:
[0023] (1) Weigh the alkyl sulfate with a weight ratio of 20% to 30%, and the ammonium lauryl sulfate with a weight ratio of 10% to 15%. 12 h 25 SO 4 NH 4 , 25% to 35% stearic acid C 18 h 36 o 2 , 8% to 12% sodium carbonate Na 2 CO 3 ; the rest is water;
[0024] (2) Alkyl sulfate, ammonium lauryl sulfate C 12 h 25 SO 4 NH 4 Add to the reaction kettle respectively,...
Embodiment 1
[0031] Example 1: This example provides a gas well high-temperature solid foaming agent SG-1.
[0032] SG-1 type high temperature solid foaming agent, it is composed of sodium lauryl sulfate C 12 h 25 SO 4 Na, ammonium lauryl sulfate C 12 h 25 SO 4 NH 4 , stearic acid C 18 h 36 o 2 , sodium carbonate Na 2 CO 3 And water composition, their percentage by weight is: sodium lauryl sulfate C 12 h 25 SO 4 Na30%, ammonium lauryl sulfate C12 h 25 SO 4 NH 4 15%, stearic acid C 18 h 36 o 2 25%, sodium carbonate Na 2 CO 3 8%, the rest is water;
[0033] (1) Weigh the sodium lauryl sulfate C with a weight ratio of 30% 12 h 25 SO 4 Na, 15% ammonium lauryl sulfate C 12 h 25 SO 4 NH 4 , 25% stearic acid C 18 h 36 o 2 , 8% sodium carbonate Na 2 CO 3 ; the rest is water;
[0034] (2) Sodium lauryl sulfate C 12 h 25 SO 4 Na, ammonium lauryl sulfate C 12 h 25 SO 4 NH 4 Add to the reaction kettle respectively, stir for 2 hours, the stirring speed is 100r / m...
Embodiment 2
[0040] Example 2: This example provides a gas well high-temperature solid foaming agent SKG-1.
[0041] SKG-1 type high temperature solid foaming agent, it is composed of sodium lauryl sulfate C 12 h 25 SO 4 Na,C 13~16 Sodium Fatty Alcohol Sulfate C 13~16 h 27~33 SO 4 Na, ammonium lauryl sulfate C 12 h 25 SO 4 NH 4 , stearic acid C 18 h 36 o 2 , sodium carbonate Na 2 CO 3 And water composition, their percentage by weight is: sodium lauryl sulfate C 12 h 25 SO 4 Na10%, C 13~16 Sodium Fatty Alcohol Sulfate C 13~16 h 27~33 SO 4 Na10%, ammonium lauryl sulfate C 12 h 25 SO 4 NH 4 10%, stearic acid C 18 h 36 o 2 35%, sodium carbonate Na 2 CO 3 12%, the rest is water;
[0042] The preparation method of SKG-1 type high temperature solid foaming agent:
[0043] (1) Weigh 10% sodium lauryl sulfate C 12 h 25 SO 4 Na, 10% C 13~16 Sodium Fatty Alcohol Sulfate C 13~16 h 27~33 SO 4 Na, 10% ammonium lauryl sulfate C 12 h 25 SO 4 NH 4 , 35% stearic aci...
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