Reinforcing film with separator
A separator and release layer technology, applied in the direction of pressure-sensitive film/sheet, film/sheet release liner, film/sheet-shaped adhesive, etc., can solve problems such as damage to optical components or electronic components, and achieve Damage mitigation effect
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manufacture Embodiment 1
[0180] [Production Example 1]: Production of (meth)acrylic polymer (1)
[0181] 95 parts by weight of butyl acrylate (manufactured by Nippon Shokubai Co., Ltd.), 5 parts by weight of acrylic acid (manufactured by Toagosei Co., Ltd.), 0.2 parts by weight of 2,2'- Azobisisobutyronitrile (manufactured by Wako Pure Chemical Industries, Ltd.), and 156 parts by weight of ethyl acetate were loaded into a four-necked flask including a stirring blade, a thermometer, a nitrogen introduction tube, and a condenser. While stirring the mixture gently, nitrogen gas was introduced into the flask. While maintaining the temperature of the liquid in the flask at about 63°C, polymerization was performed for 10 hours. Thus, a solution (40% by weight) of a (meth)acrylic polymer (1) having a weight average molecular weight of 700,000 was prepared.
manufacture Embodiment 2
[0182] [Production Example 2]: Production of (meth)acrylic polymer (2)
[0183] 95 parts by weight of cyclohexyl methacrylate (glass transition temperature of homopolymer (polycyclohexyl methacrylate): 66° C.) and 5 parts by weight of acrylic acid serving as a chain transfer agent were used as monomer components. 3 parts by weight of 2-mercaptoethanol, 0.2 parts by weight of 2,2′-azobisisobutyronitrile serving as a polymerization initiator, and 103.2 parts by weight of toluene serving as a polymerization solvent were loaded into a separable flask, and The mixture was stirred for 1 hour while nitrogen gas was introduced into the flask. After oxygen in the polymerization system had been removed as described above, the temperature in the system was raised to 70°C, and the mixture was allowed to react for 3 hours. Further, the mixture was reacted at 75° C. for 2 hours. Thus, a solution (50% by weight) of a (meth)acrylic polymer (2) having a weight average molecular weight of 4,0...
manufacture Embodiment 3
[0184] [Manufacture Example 3]: Manufacture of acrylic adhesive composition (1)
[0185] To the solution of the (meth)acrylic polymer (1) obtained in Production Example 1, TETRAD-C (manufactured by Mitsubishi Gas Chemical Company, Inc.) serving as a crosslinking agent was added. The quantity of this crosslinking agent is 0.075 weight part by solid content with respect to 100 weight part of solid content of the solution of the (meth)acryl-type polymer (1). The mixture was diluted with ethyl acetate so that the total solid content became 25% by weight, followed by stirring with a disperser. Thus, an acrylic adhesive composition (1) containing an acrylic resin was obtained.
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