Polarizing plate
A polarizing plate and polarizing film technology, applied in polarizing elements, applications, instruments, etc., can solve the problems of easy cracking and low resistance of polarizing films
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[0232] Hereinafter, although an Example and a comparative example are shown and this invention is demonstrated more concretely, this invention is not limited to these examples. Hereinafter, parts and % showing the usage amount or content are based on weight unless otherwise specified.
[0233] The thicknesses of the thermoplastic resin film, the polarizing film, and the adhesive layer, the tensile elastic modulus of the thermoplastic resin film, and the storage elastic modulus of the adhesive layer were measured according to the following method.
[0234] (1) Thickness of thermoplastic resin film and polarizing film
[0235] A strip-shaped test piece whose MD length is 50 mm×TD length is the total width is cut out from the film. Next, the thickness of the film was measured at intervals of 100 mm in the film width direction using a digital micrometer "MH-15M" manufactured by Nikon Corporation. Let the average value of the obtained measured values be thickness [mm].
[0236...
manufacture example 1
[0240] (Manufacturing example 1: Preparation of active energy ray-curable adhesive)
[0241] After mixing the cationic curable component (A) and the cationic polymerization initiator (B) shown in Table 1, defoaming was performed to prepare an adhesive as an active energy ray curable adhesive (ultraviolet curable adhesive). Agents 1 and 2. The unit of the compounding quantity of each component in Table 1 is "part".
[0242] [Table 1]
[0243]
[0244] The details of each component shown in Table 1 are as follows.
[0245] [1] Epoxy compound A1-1: special novolak type epoxy resin "157S20" manufactured by Mitsubishi Chemical Corporation,
[0246] [2] Epoxy compound A1-2: neopentyl glycol diglycidyl ether [Z=-CH in the above formula (III) 2 C(CH 3 ) 2 CH 2 -compound of],
[0247] [3] Epoxy compound A1-3: Weight average molecular weight obtained by radically polymerizing a monomer composition composed of 25 parts of glycidyl methacrylate (GMA) and 75 parts of methyl meth...
manufacture example 2
[0250] (Manufacturing example 2: Production of polarizing film)
[0251] A polyvinyl alcohol film manufactured by Kuraray (“PE6000” manufactured by Kuraray Co., Ltd.) was conveyed continuously, and immersed in a swelling bath made of pure water at 20° C. for a residence time of 31 seconds (swelling step). Thereafter, the membrane pulled out from the swelling bath was immersed in a 30° C. dyeing bath containing iodine having a potassium iodide / water ratio of 2 / 100 (weight ratio) for a residence time of 122 seconds (dyeing step).
[0252] Next, the film pulled out from the dyeing bath was immersed in a cross-linking bath at 56° C. with a residence time of 70 seconds in potassium iodide / boric acid / water of 12 / 4.1 / 100 (weight ratio), and then immersed in a crosslinking bath with a residence time of 13 seconds in Potassium iodide / boric acid / water is 9 / 2.9 / 100 (weight ratio) cross-linking bath at 40° C. (cross-linking step). In the dyeing step and the crosslinking step, longitudina...
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