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Manufacturing method of nanometer low-porosity porous aluminum alloy

An aluminum alloy and porosity technology, which is applied in the field of preparing a micron-scale low-porosity porous aluminum alloy by sintering and dissolution method, can solve the problems that cannot meet the requirements of porosity and pore size, and achieve cost saving, flexible operation, and preparation The effect of simple process

Active Publication Date: 2018-03-13
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

To sum up, the existing preparation methods have various limitations and cannot meet the requirements of porosity and pore size under specific conditions.

Method used

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  • Manufacturing method of nanometer low-porosity porous aluminum alloy
  • Manufacturing method of nanometer low-porosity porous aluminum alloy
  • Manufacturing method of nanometer low-porosity porous aluminum alloy

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049]The matrix powder selected is 2A12 aluminum alloy powder. First, the water-soluble pore former powder with a particle size distribution of 15-40 μm and the 2A12 aluminum alloy powder with a particle size distribution of 10-20 μm were dried in a drying oven at 80° C. for 5 hours. Mix 2A12 powder and water-soluble pore-forming agent powder according to the volume fraction of 7:3 (that is, the value of A is 30), and then mix them in a three-dimensional mixer for 3 hours, and the speed of the mixer is 20r / min. Take it out and save it for later use. Put the composite powder in the mold to form the prefabricated body at 200MPa, hold the pressure for 20s, and prepare the prefabricated body. The prefabricated green body is subjected to 600° C. in a vacuum sintering furnace for a holding time of 180 minutes to prepare a sintered body. The porous aluminum alloy was prepared by removing the pore-forming agent from the sintered body prepared by the powder metallurgy technology by ...

Embodiment 2

[0051] The matrix powder selected is 2A12 aluminum alloy powder. First, the water-soluble pore former powder with a particle size distribution of 15-40 μm and the 2A12 aluminum alloy powder with a particle size distribution of 10-20 μm were dried in a drying oven at 80° C. for 5 hours. The 2A12 powder and the water-soluble pore-forming agent powder are mixed according to the volume fraction of 13:7 (that is, the value of A is 35), and then mixed in a three-dimensional mixer for 3 hours, and the speed of the mixer is 20r / min, and then in a vacuum environment Take it out and save it for later use. Put the composite powder in the mold to form the prefabricated body at 200MPa, hold the pressure for 20s, and prepare the prefabricated body. The prefabricated green body is subjected to 600° C. in a vacuum sintering furnace for a holding time of 180 minutes to prepare a sintered body. The porous aluminum alloy was prepared by removing the pore-forming agent from the sintered body pr...

Embodiment 3

[0053] The matrix powder selected is 2A12 aluminum alloy powder. First, the water-soluble pore former powder with a particle size distribution of 15-40 μm and the 2A12 aluminum alloy powder with a particle size distribution of 10-20 μm were dried in a drying oven at 80° C. for 5 hours. Mix 2A12 powder and water-soluble pore-forming agent powder according to the volume ratio of 6:4 (that is, the value of A is 40), and then mix them in a three-dimensional mixer for 3 hours, and the speed of the mixer is 20r / min, and then under vacuum environment Take it out and save it for later use. Put the composite powder in the mold to form the prefabricated body at 200MPa, hold the pressure for 20s, and prepare the prefabricated body. The prefabricated green body is subjected to 600° C. in a vacuum sintering furnace for a holding time of 180 minutes to prepare a sintered body. The porous aluminum alloy was prepared by removing the pore-forming agent from the sintered body prepared by the ...

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Abstract

The invention relates to a manufacturing method of a nanometer low-porosity porous aluminum alloy, and in particular relates to a method for manufacturing the nanometer low-porosity porous aluminum alloy by treating a water-soluble pore forming agent as a porosity controlling agent and utilizing a sintering and dissolving method. The manufacturing method comprises the following steps: setting theporosity of the porous aluminum alloy to be A%; preparing the water-soluble pore forming agent powder and aluminum alloy powder based on the volume ratio of A%: (1-A%), and uniformly mixing to obtainmixed powder; pressing and molding; and sintering under the temperature of 550-650 DEG C in a vacuum environment to obtain a sintering body; soaking the sintering body in a water solution; and dryingto obtain the porous aluminum alloy with the porosity of B%, wherein the relation of B and A sees the description. The method is simple in processes, and applicable to the manufacturing of low-porosity micron-aperture porous aluminum alloy; the porosity and the pore diameter can be effectively controlled; the operation is flexible; and massive industrial application is conveniently carried out.

Description

technical field [0001] The invention relates to a method for preparing a micron-scale porous aluminum alloy with low porosity, in particular to a method for preparing a micron-scale low-porosity porous aluminum alloy by using a water-soluble pore-forming agent as a porosity control agent and adopting a sintering dissolution method . Background technique [0002] As a kind of porous material, porous aluminum alloy has structural characteristics that can realize the diversification of functions, and is widely used in electrode materials, automobiles, aerospace, catalysis, heat exchange and other fields. However, the porous aluminum alloys currently prepared have large pore sizes, which are difficult to fine-tune and control, and due to their performance degradation, the integration of their structure and function cannot be realized when they are used as structural parts in specific environments. The biggest feature of the micron-sized porous aluminum alloy prepared by modern ...

Claims

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Application Information

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IPC IPC(8): C22C1/08C22C21/00B22F3/11
Inventor 马运柱刘超刘文胜史政刘阳龙路平
Owner CENT SOUTH UNIV