Dyeing method of natural fiber

A natural fiber and dyeing method technology, applied in the field of natural fiber dyeing, can solve the problems of losing the main advantages of anhydrous supercritical carbon dioxide dyeing, weak interaction between natural plant dyes and cotton fibers, poor fastness, etc., and achieve good Social benefits, excellent reproducibility and high efficiency

Inactive Publication Date: 2018-05-01
JIANGSU NEW REBA TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the interaction between natural vegetable dyes and cotton fibers is weak, and there are problems of low color depth and poor fastness after dyeing cotton fibers, which limits the application of natural vegetable dyes in supercritical carbon dioxide cotton fiber dyeing technology.
[0006] At present, most of the dyeing experiments of natural fibers require pretreatment, and sometimes the fibers need to be washed in water or solvent after dyeing to remove the pre-impregnated substances on the fiber surface, thus losing the ability of anhydrous supercritical carbon dioxide dyeing. The main advantage, in addition to the additional energy-intensive treatment and drying steps of the fibers that are unnecessary in conventional aqueous dyeing

Method used

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  • Dyeing method of natural fiber

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Experimental program
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Effect test

Embodiment 1

[0035] This embodiment discloses a method for dyeing natural fibers utilizing supercritical carbon dioxide fluid, and the specific steps are as follows:

[0036] Step 1. Extract 1g of natural plant dyes to 80 mesh in a fineness extractor, add liquid carbon dioxide and dimethylformamide into the supercritical carbon dioxide dyeing device, heat to 105°C, and keep for 30 minutes, then add natural fibers In the supercritical carbon dioxide dyeing device, dyeing is carried out at a temperature of 150° C. and a pressure of 25 MPa for 100 minutes. The mass ratio of the natural vegetable dye to the natural fiber is 1:10. Described fixing agent is 15g / L.

[0037] Step 2, controlling the supercritical carbon dioxide dyeing device to release the pressure, and recovering the carbon dioxide and the natural plant dye under the conditions of a temperature of 25-35° C. and a pressure of 4-6 MPa.

[0038] Step 3: Control the supercritical carbon dioxide dyeing device to release the pressure,...

Embodiment 2

[0043] This embodiment discloses a method for dyeing natural fibers utilizing supercritical carbon dioxide fluid, and the specific steps are as follows:

[0044] Step 1. Extract 1g of natural plant dyes to 100 mesh in a fineness extractor, add liquid carbon dioxide and ethylenediamine to the supercritical carbon dioxide dyeing device, heat to 125°C, and keep for 20 minutes, then add natural fibers to the supercritical carbon dioxide dyeing device. In the critical carbon dioxide dyeing device, dyeing is carried out under the conditions of a temperature of 130° C. and a pressure of 24 MPa, and is maintained for 90 minutes. The mass ratio of the natural vegetable dye to the natural fiber is 1:7. Described fixing agent is 12g / L.

[0045] Step 2, controlling the supercritical carbon dioxide dyeing device to release the pressure, and recovering the carbon dioxide and the natural plant dye under the conditions of a temperature of 25-35° C. and a pressure of 4-6 MPa.

[0046] Step 3...

Embodiment 3

[0050]This embodiment discloses a method for dyeing natural fibers utilizing supercritical carbon dioxide fluid, and the specific steps are as follows:

[0051] Step 1. Extract 1g of natural plant dyes to 100 mesh in a fineness extractor, add liquid carbon dioxide and diethylenetriamine into the supercritical carbon dioxide dyeing device, heat to 107°C, and keep for 30 minutes, then add natural fibers to the In the supercritical carbon dioxide dyeing device, the dyeing was carried out at a temperature of 140° C. and a pressure of 20 MPa, and was maintained for 110 minutes. The natural plant dye described in the present embodiment is turmeric dye, and described natural fiber is cotton fiber. The mass ratio of the natural vegetable dye to the natural fiber is 1:5. Described fixing agent is 10g / L.

[0052] Step 2, controlling the supercritical carbon dioxide dyeing device to release the pressure, and recovering the carbon dioxide and the natural plant dye under the conditions o...

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Abstract

The invention discloses a dyeing method of a natural fiber. The dyeing method comprises the following particular steps of firstly, adding natural vegetable dye, liquid carbon dioxide and a color fixing agent into a supercritical carbon dioxide dyeing device, heating, and maintaining for a certain time; afterwards, adding the natural fiber into the supercritical carbon dioxide dyeing device, dyeingat and under certain temperature and pressure, and maintaining for a certain time; next, relieving the pressure, cooling to a normal temperature and depressurizing to normal pressure to obtain a preliminarily dyed natural fiber; treating the preliminarily dyed natural fiber, afterwards, adding into the supercritical carbon dioxide dyeing device, dyeing at and under certain temperature and pressure, maintaining for a certain time, and then relieving the pressure to obtain a finished-product dyed natural fiber. The dyeing method, through a two-step dyeing method, is used for realizing printingand dyeing the natural fiber by natural dye, and further, does not need pretreatment, and the dyeing method has advantages of good environmental protection effect, water resource conservation, good color fixation effect and the like.

Description

technical field [0001] The invention relates to the technical field of natural fiber dyeing, in particular to a natural fiber dyeing method. Background technique [0002] Supercritical carbon dioxide fluid is a green and environment-friendly fluid medium. It replaces the traditional water bath for dyeing and processing fiber textiles. It has the characteristics of environmental protection and clean production, as well as outstanding energy-saving and consumption-reducing effects. The status quo of high resource consumption, large amount of sewage discharge, and serious environmental pollution is of great significance. [0003] At present, synthetic fiber textiles such as polyester, nylon, acetate, and acrylic can be dyed satisfactorily by using hydrophobic disperse dyes in supercritical carbon dioxide fluid. However, the supercritical carbon dioxide fluid dyeing of hydrophilic natural fibers, such as cotton, real silk, wool and other fiber textiles, which account for a larg...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/34D06P1/94D06P1/00D06P3/60
Inventor 储平徐有琦
Owner JIANGSU NEW REBA TECH CO LTD
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