A kind of lightweight thermal fiber and preparation method thereof
A heat-retaining fiber and lightweight technology, which is applied in the direction of fiber processing, fiber type, fiber chemical characteristics, etc., can solve the problems of fiber extrusion speed difference, inconsistent pressure drop, and affect the smooth progress of fiber spinning processing, so as to improve the strength, Improved compatibility and excellent thermal stability
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Embodiment 1
[0066] A lightweight thermal fiber, the preparation method of which is:
[0067] (1) preparation of oiling agent for oiling;
[0068] Mix 2-hydroxymethyl-12-crown-4 with potassium dodecyl phosphate, trimethylolpropane laurate and sodium hexadecylsulfonate at room temperature and add to 12# mineral oil and uniformly stirred at 40°C for 2.5h to obtain an oil agent; the addition amount of each component is as follows in parts by weight: 5 parts of 12# mineral oil; 95 parts of 2-hydroxymethyl-12-crown-4; 12 9 parts of potassium alkyl phosphate; 2 parts of sodium hexadecyl sulfonate. The content of crown ether in the prepared oil is 85.58wt%. The oil has excellent high temperature resistance. After heat treatment at 200°C for 2 hours, the thermal weight loss is 9wt%. The viscosity of the oil is low. When the kinematic viscosity is 29.5mm 2 / s, the kinematic viscosity after the concentration of 10wt% emulsion is configured with water is 0.93mm 2 / s, the oil film strength of the ...
Embodiment 2
[0073] A lightweight thermal fiber, the preparation method of which is:
[0074](1) Preparation of oiling agent for oiling; 15-crown ether-5 and isomeric tridecyl alcohol polyoxyethylene ether phosphate potassium salt, trimethylolpropane laurate and sodium dodecylsulfonate are mixed at room temperature After mixing evenly, add it to 13# mineral oil and stir evenly at 52°C for 2 hours to obtain an oil agent; in parts by weight, the addition amount of each component is as follows: 10 parts of 13# mineral oil; trimethylolpropane lauric acid 5 parts of ester; 70 parts of 15-crown ether-5; 8 parts of isomeric tridecyl polyoxyethylene ether phosphate potassium salt; 6 parts of sodium dodecylsulfonate. The content of the crown ether in the prepared oil is 70.70wt%. The high temperature resistance of the oil is excellent. After heat treatment at 200°C for 2 hours, the thermal weight loss is 13.5wt%. The viscosity of the oil is low, at (50 ± 0.01) At ℃, the kinematic viscosity is 28.6...
Embodiment 3
[0079] A lightweight thermal fiber, the preparation method of which is:
[0080] (1) Oil preparation for oiling; 2-hydroxymethyl-15-crown-5 and potassium salt of tetradecyl phosphate, trimethylolpropane laurate and sodium pentadecylsulfonate After mixing evenly at room temperature, add it to 11# mineral oil and stir evenly at 48°C for 3 hours to obtain an oil agent; in parts by weight, the addition amount of each component is as follows: 8 parts of 11# mineral oil; trimethylolpropane lauryl 10 parts of acid ester;
[0081] 2-Hydroxymethyl-15-crown-585 parts; Tetradecyl phosphate potassium salt 11 parts; Sodium pentadecylsulfonate 5 parts. The content of crown ether in the prepared oil is 70.83wt%. The oil has excellent high temperature resistance. After heat treatment at 200°C for 2 hours, the thermal weight loss is 11wt%. The viscosity of the oil is low. When the kinematic viscosity is 30.1mm 2 / s, the kinematic viscosity after the concentration is 10wt% emulsion configure...
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