A kind of organic synthesis catalyst equipment

Abstract

The invention discloses novel equipment for organically synthesizing a novel catalyst. The novel equipment comprises a mixing tank, a reaction tower and an MTBE storage tank, wherein stable input systems are symmetrically arranged at the front and rear ends of the left side of the mixing tank and comprise gas storage tanks; and a pressurizing tank is fixedly connected to the right end of each connecting pipe, a fixed motor is arranged outside the pressurizing tank, and a pressure maintaining space is formed in each pressure maintaining tank; and a reaction fractionation space is formed in a reaction tower, and a distilling pipe is fixedly connected to the center of the upper end surface of the reaction tower. When the novel equipment works and the flow rate of gas exceeds the standard, gaspushes a sealing plate to move backwards, and redundant gas flows back to the gas storage space through a decompression hole, so that the mixing proportion of gas is guaranteed; the mixed liquid of C4 and methanol is vaporized during the reaction by virtue of heat produced during the reaction, partial gas mixture is discharged through a distilling hole so as to bring away a large number of heat,so that the situation that equipment is burnt due to the over-high temperature in the reaction fractionation space is prevented.

Description

technical field [0001] The invention relates to the field of catalyst synthesis, in particular to an organic synthesis catalyst device. Background technique [0002] At present, methyl tert-butyl ether is called MTBE for short. As a gasoline catalyst to increase the octane number of gasoline, its manufacturing method has been widely used in the process of petrochemical production. In the process of preparing MTBE, methanol and Carbon four is used as a raw material, and the mixing ratio of methanol and carbon four is very important in the production process. At present, in production, it is prepared and then put into the reactor for catalytic reaction, which wastes a lot of time and money. Moreover, my country's production The MTBE process generally adopts a fixed reaction bed, which reacts in a liquid phase state, and the reaction generates a large amount of heat. Therefore, a tubular reactor or a cylindrical reactor cooled by external circulation of the reaction material is u...

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Problems solved by technology

[0002] At present, methyl tert-butyl ether is called MTBE for short. As a gasoline catalyst to increase the octane number of gasoline, its manufacturing method has been widely used in the process of petrochemical production. In the process of preparing MTBE, methanol and Carbon four is used as a raw material, and the mixing ratio of methanol and carbon four is very important in the production process. At present, in production, it is prepared and then put into the reactor for catalytic reaction, which wastes a lot of time and money. Moreover, my country's production The MTBE process generally adopts a fixed reaction bed, which reacts in a liquid phase state, and the reaction generates a large amount of heat. Therefore, a tubular reactor or a cylindrical reactor cooled by external circulation of the reaction material is used. The equipment is complicated, the investment is large, and the energy consumption is large. High, during the reaction process, methanol and carbon four are azeotropic, and MTBE is a heavy component, which can be produced by reactive fractionation, that is, liquid phase and gas phase react at the same time, and distill while reacting

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