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Secondary decoloring method of animal and vegetable oil

A secondary decolorization, animal and vegetable oil technology, applied in the direction of fat oil/fat refining, fat production, etc., can solve the problems such as the decolorization and adsorption function of waste clay is not fully utilized, the adsorption of soap and phospholipids by fresh clay is reduced, and the filter layer channel is easily blocked. To achieve the effect of reducing the number of blowing cakes, improving the secondary utilization rate and good adsorption function

Active Publication Date: 2018-07-06
立钢贝纳德工程设备(广州)有限公司
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  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Disadvantages of this process: the decolorization and adsorption function of waste clay is not fully utilized, and the utilization rate of waste clay is low
[0006] There is not much difference between the re-decolorization process technology equipment and the conventional process technology, except that there are slightly more filters. The process is: after the first driving, fresh clay and heated oil are mixed evenly, and then 100 in the decolorization tower under vacuum conditions. After staying at -110°C for a certain period of time, it is transported to the leaf filter by the filter feed pump for filtration and separation. When the filter reaches the set pressure, switch the oil to be decolorized to the spare filter to continue filtering. The oil to be decolorized Adjust to the filter that has been filled with clay, and use the filter cake to pre-decolorize the phospholipids, neutralized residual soap, and some pigments in the raw materials. After the decolorized oil passes through the filter filled with clay, the oil enters the oil clay mixing tank for pre-fresh After the filter pressure of the decolorized oil and the filter cake that has formed a filter cake reaches a certain value, switch to another filter filled with clay to filter, and the filter that has reached the filter pressure is passed into a certain steam pressure. The oil is emptied and the filter cake is blown dry, such as the conventional decolorization process: the filter cake is blown dry and then discharged from the filter, and concentrated for waste solid treatment; the advantage of this process: the phospholipids and soaps in the oil to be decolorized are decolorized by using the waste clay in the leaf filter. And part of a small amount of pigment adsorption, reduce the adsorption of soap and phospholipids by fresh clay, and increase the decolorization and adsorption function of fresh clay; Disadvantages: 1. Because the filter layer of waste clay has been formed, waste clay preferentially adsorbs soap or phospholipids, and it is easy to absorb in the filter layer close to the saturation of adsorption Further accumulation of soap or phospholipids on the surface will easily block the channel of the filter layer, further increase the filtration pressure and have to stop the filtration; 2. The waste clay cannot be evenly contacted with the fresh oil, so that the adsorption function cannot be fully exerted, and the efficiency is low

Method used

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  • Secondary decoloring method of animal and vegetable oil

Examples

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Effect test

Embodiment 1

[0037] The secondary decolorization device for animal and vegetable oils includes a pre-decolorization tower, a primary filter, a decolorization tower, a secondary filter, a bag filter, and a pump. Along the flow direction of the material, the pre-bleaching tower, pump, primary filter, decolorizing tower, pump, secondary filter, and bag filter are connected in sequence, and the secondary filter, pump, and pre-bleaching tower are connected in sequence.

[0038] The primary filter is a leaf filter.

[0039]The decolorized oil is mixed with acid, enters the degumming tank and stays for a certain period of time, and then mixes it with the once-used waste clay oil mixture separated by filtration after decolorization, enters the pre-decolorization tower, and vacuums at a temperature of 60-70mbar and a temperature of 105- Stay at 110°C for a certain period of time under steam stirring conditions, and use a decolorization pump to transport the mixture to a primary filter for separatio...

Embodiment 2

[0042] The present embodiment is the secondary decolorization method of neutralizing rapeseed oil, specifically comprises the following steps:

[0043] (1) Neutralized rapeseed oil is heated to a temperature of about 85°C through a heat exchanger, mixed with a certain amount of citric acid, then enters the dry degumming mixer, stays in the mixer for a certain period of time, enters the pre-decolorization tower, and passes through the decolorization tower and The once-used waste clay separated by the secondary filter is mixed, and the mixture is heated to 100-110°C in the pre-bleaching tower, and the vacuum pressure is 65mbar.

[0044] (2) During the initial start-up, the neutralized rapeseed oil enters the oil clay mixer directly from the dry degumming mixer, mixes with fresh clay, and then overflows to the decolorization tower. The initial decolorization clay is added in an amount of 2% oil weight, and is heated and stopped in the bleaching tower After a certain period of tim...

Embodiment 3

[0051] The present embodiment is the secondary decolorization method of crude palm oil, specifically comprises the following steps:

[0052] (1) Crude palm oil is heated to a temperature of about 85°C through a heat exchanger, mixed with a certain amount of citric acid, then enters a dry degumming mixer, stays in the mixer for a certain period of time, enters a pre-decolorization tower, and passes through a decolorization tower and a secondary The once-used waste clay separated by the filter is mixed, and the mixture is heated to 100-110°C in the pre-bleaching tower, and the vacuum pressure is 65mbar.

[0053] (2) The crude palm oil from the dry degumming mixer in the initial driving directly enters the oil clay mixer and is mixed with fresh clay and then overflows to the decolorization tower. Finally, in order to do a comparison experiment, the oil is directly input into the primary filter according to the conventional process, and the oil after the primary filter passes thro...

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Abstract

The invention relates to a secondary decoloring method of animal and vegetable oil. The secondary decoloring method comprises the following steps of a, mixing oil to be decolored and primarily used waste clay, and enabling a mixture to enter a decoloring tower for decoloring treatment; b, treating a material discharged in the step 1 with a primary filter to obtain primarily decolored oil and secondarily used waste clay, and treating the collected secondarily used waste clay according to a conventional waste treatment technology; c, mixing the primarily decolored oil obtained in the step b andnew clay, and enabling a mixture to enter the decoloring tower for decoloring treatment; d, treating a material discharged in the step c with a secondary filter to obtain secondarily decolored oil andprimarily used waste clay, enabling the primarily used waste clay to reflux to the step a for use; and e, treating the secondarily decolored oil obtained in the step d with a bag filter to obtain decolored oil. The secondary decoloring method of the animal and vegetable oil enables the secondary utilization ratio of waste clay to be increased, the waste clay and oil to be more fully mixed and theuse ratio of fresh clay to be lowered and belongs to the technical field of animal and vegetable oil decoloring.

Description

technical field [0001] The invention relates to the decolorization technology of animal and vegetable oils, in particular to a secondary decolorization method of animal and vegetable oils. Background technique [0002] The methods currently used for decolorization of animal and vegetable oils are: conventional decolorization process and pre-decolorization process. [0003] Conventional decolorization process: [0004] Conventional animal and vegetable oil decolorization process: After mixing fresh white clay and heated oil evenly, stay in the decolorization tower for a certain period of time at about 100-110°C under vacuum conditions, and then transport it to the filter through the filter feed pump for filtration and separation. After the filtration pressure of the filter reaches the set value, the steam pressure is introduced to discharge the oil in the filter. After the oil is emptied, the filter cake clay is blown dry by steam and discharged from the filter, where it is ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B3/00C11B3/10
CPCC11B3/001C11B3/008C11B3/10
Inventor 陈清明程玉龙张建利
Owner 立钢贝纳德工程设备(广州)有限公司
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