Melt-spinning spinneret device and use method thereof
A technology of melt spinning and spinneret, which is applied in the direction of melt spinning, spinneret assemblies, textiles and papermaking, etc. It can solve the problems of high broken filament rate, poor quality of precursor filament, and large difference in fiber precursor diameter, etc. problem, to achieve the effect of ensuring uniformity, improving quality and good controllability
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Embodiment 1
[0015] The spinneret area 1 of the circular spinneret is in the form of a concentric ring, evenly distributed on the outer circumference of the circular spinneret, and is divided into four by grooves, and the spinneret area is composed of a plurality of arranged spinneret 4 Composition, the outer groove of each spinneret hole area is the heating compensation area, the groove of the heating compensation area is passed into the circulation heat transfer oil or filled with the heater, the groove is provided with the heat transfer oil inlet and outlet or the heater wire inlet and outlet 5, spray The hole area 1 and the heating compensation area 2 are completely separated by a hard sealing surface 3 .
[0016] The heat-sensitive naphthalene-based synthetic mesophase pitch with a softening point of 280° C. is melt-spun by using the melt-spinning spinneret designed in the present invention. Connect the spinneret to the spinning box, and after the temperature of the spinning box reach...
Embodiment 2
[0018] The heat-sensitive petroleum-based mesophase pitch with a softening point of 295° C. is melt-spun by using the melt-spinning spinneret designed in the present invention. Connect the spinneret to the spinning box, and after the temperature of the spinning box reaches the set temperature of 345°C and keep it warm for 2 hours, turn on the high-temperature circulating heat transfer oil, the flow rate of the heat transfer oil is 10L / min, and the temperature is 345°C, test the spinneret hole area through the far-infrared temperature, and start spinning when the temperature of the spinneret plate surface reaches 345±1°C. The mesophase pitch-based carbon fiber comes out of the spinneret, and after oiling, bundling, drawing, and winding, continuous high-quality mesophase pitch-based carbon fiber precursors can be obtained. Using the above-mentioned spinneret to carry out the melt spinning of the mesophase pitch, the broken filament rate can be controlled at 0.15%, and the diamet...
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