Herbicide composition of penoxsulam and pyriminobac-methyl
A technology of penoxsulam and pyrifluramid, which is applied in the field of pharmaceutical compounds, can solve the problems of non-weed biological hazards, soil pollution, water quality degradation, etc., and achieve the effects of high residual effect, less pollution, and fewer reaction steps
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Embodiment 1
[0021] Embodiment 1: as figure 1 As shown, the present invention provides a herbicide composition of penoxsulam and pyriflubac, which is characterized in that: the formula is composed of penoxsulam, pyrimifluben, pyrazosulfuron-methyl, oxazicone, Pretilachlor, quinclorac, and pyrazosulfuron-methyl, the formula is made of the following raw materials in parts by weight: 5 parts of penoxsulam, 8 parts of pyrifluramid, 5 parts of chlorpyrazosulfuron-methyl, oxazicine Ketone 10 parts, pretilachlor 1 part, quinclorac 10 parts and pyrazosulfuron-methyl 6 parts.
[0022] According to the above technical scheme, the preparation method of penoxsulam uses methyl 2-methoxyacetate as the starting material, reacts with methyl formate and sodium methoxide to obtain methyl 3-hydroxy-2-methoxyacrylate The sodium salt of the ester, then reacted with methylisothiourea to give 2,5-dimethoxy-4-hydroxypyrimidine, followed by chlorination with phosphorus oxychloride to give 4-chloro-2,5-dimethoxypy...
Embodiment 2
[0031] Embodiment 2: as figure 1 As shown, the present invention provides a herbicide composition of penoxsulam and pyriflubac, which is characterized in that: the formula is composed of penoxsulam, pyrimifluben, pyrazosulfuron-methyl, oxazicone, Pretilachlor, quinclorac, and pyrazosulfuron-methyl, the formula is made of the following raw materials in parts by weight: 8 parts of penoxsulam, 9 parts of pyriflun-methyl, 7 parts of chlorpyrazosulfuron-methyl, oxazicine ketone 12 parts, pretilachlor 3 parts, quinclorac 11 parts and pyrazosulfuron-methyl 8 parts.
[0032] According to the above technical scheme, the preparation method of penoxsulam uses methyl 2-methoxyacetate as the starting material, reacts with methyl formate and sodium methoxide to obtain methyl 3-hydroxy-2-methoxyacrylate The sodium salt of the ester, then reacted with methylisothiourea to give 2,5-dimethoxy-4-hydroxypyrimidine, followed by chlorination with phosphorus oxychloride to give 4-chloro-2,5-dimethoxy...
Embodiment 3
[0041] Embodiment 3: as figure 1 As shown, the present invention provides a herbicide composition of penoxsulam and pyriflubac, which is characterized in that: the formula is composed of penoxsulam, pyrimifluben, pyrazosulfuron-methyl, oxazicone, Pretilachlor, quinclorac, and pyrazosulfuron-methyl, the formula is made of the following raw materials in parts by weight: 10 parts of penoxsulam, 10 parts of pyrifluramid, 15 parts of clopyrazosulfuron-methyl, oxazicine Ketone 15 parts, pretilachlor 5 parts, quinclorac 15 parts and pyrazosulfuron-methyl 10 parts.
[0042] According to the above technical scheme, the preparation method of penoxsulam uses methyl 2-methoxyacetate as the starting material, reacts with methyl formate and sodium methoxide to obtain methyl 3-hydroxy-2-methoxyacrylate The sodium salt of the ester, then reacted with methylisothiourea to give 2,5-dimethoxy-4-hydroxypyrimidine, followed by chlorination with phosphorus oxychloride to give 4-chloro-2,5-dimethox...
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