Film for pressure sensing test and preparation method of film
A technology of induction testing and film, which is applied in the direction of measuring fluid pressure, measuring force, measuring device, etc., to achieve the effects of simple preparation process, convenient use and low cost
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Embodiment 1
[0062] 1. Preparation of microspheres:
[0063] a) Dissolve 3g of urea in 24.892g of deionized water, then add 8.108g, 37wt% formaldehyde aqueous solution, stir evenly, add 10wt% triethanolamine aqueous solution to adjust the pH value of the solution to 8.5, then react at 70°C for 1 hour to prepare Obtain urea-formaldehyde resin prepolymer;
[0064] b) Dissolve 0.4g sodium dodecyl sulfate (SDS, emulsifier), 0.12g cetyl alcohol (CA, stabilizer) in 30g deionized water, add 6g solvent oil (diarylethane) after fully dissolving , the resulting mixture was placed in an ultrasonic disperser at room temperature (about 25° C.) and subjected to ultrasonic treatment for 5 minutes (ultrasonic output power was 60%) to obtain an emulsion for polymerization;
[0065] c) mixing the urea-formaldehyde resin prepolymer prepared in step a) with the polymerization emulsion prepared in step b) to obtain a mixed solution, then adopting 10wt% citric acid aqueous solution to adjust the pH value of th...
Embodiment 2
[0074] 1. Preparation of microspheres:
[0075] a) Dissolve 2 g of urea in 26.585 g of deionized water, then add 5.405 g of 37 wt % formaldehyde aqueous solution, stir evenly, add 10 wt % triethanolamine aqueous solution to adjust the pH value of the solution to 8.5, and then react at 70 ° C for 1 hour to prepare Obtain urea-formaldehyde resin prepolymer;
[0076] b) Dissolve 0.4g sodium dodecyl sulfate (SDS, emulsifier), 0.12g cetyl alcohol (CA, stabilizer) in 30g deionized water, add 8g solvent oil (diarylethane) after fully dissolving , the resulting mixture was placed in an ultrasonic disperser at room temperature (about 25° C.) and subjected to ultrasonic treatment for 5 minutes (ultrasonic output power was 60%) to obtain an emulsion for polymerization;
[0077] c) mixing the urea-formaldehyde resin prepolymer prepared in step a) with the polymerization emulsion prepared in step b) to obtain a mixed solution, then adopting 10wt% citric acid aqueous solution to adjust the...
Embodiment 3
[0086] 1. Preparation of microspheres:
[0087] a) Dissolve 2.4g of urea in 25.914g of deionized water, then add 6.486g, 37wt% formaldehyde aqueous solution, stir evenly, add 10wt% triethanolamine aqueous solution to adjust the pH value of the solution to 8.5, then react at 70°C for 1 hour, Prepare urea-formaldehyde resin prepolymer;
[0088] b) Dissolve 0.4g sodium dodecyl sulfate (SDS, emulsifier), 0.12g cetyl alcohol (CA, stabilizer) in 30g deionized water, add 8g solvent oil (diarylethane) after fully dissolving , the resulting mixture was placed in an ultrasonic disperser at 30°C for ultrasonic treatment for 5 minutes (ultrasonic output power was 65%) to obtain an emulsion for polymerization;
[0089] c) mixing the urea-formaldehyde resin prepolymer prepared in step a) with the polymerization emulsion prepared in step b) to obtain a mixed solution, then adopting 10wt% citric acid aqueous solution to adjust the pH value of the solution to 2, and then at 70 After reacting...
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