Inorganic hydrated salt phase change material and preparation method thereof
A phase-change energy storage material and inorganic hydrated salt technology, which is applied in heat exchange materials, chemical instruments and methods, etc., can solve the problem of supercooling of inorganic phase-change materials and shorten the service life of inorganic hydrated-salt phase-change materials. , limiting the application range of phase change materials and other issues, to achieve the effect of eliminating supercooling, less demanding instrument conditions, and no potential safety hazards
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Embodiment 1
[0024] The preparation method of inorganic hydrated salt phase change energy storage material at 10°C is as follows:
[0025] Calculated by the weight of the total amount of 100g, take 74.5g sodium sulfate decahydrate as inorganic hydrated salt, 8.5g xanthan gum as adhesive, 4.5g expanded graphite as thermal conductivity agent, and 4.5g sodium hexametaphosphate as modifier , 8g nanoscale material (ZrB 2 , SiO 2 and SiB 6 ) as a nucleating agent, magnetically stirred in a constant temperature water bath at 60°C for 1 hour until completely melted, and the prepared inorganic hydrate salt phase change energy storage material was packaged and stored in a packaging machine for future use.
[0026] The inorganic hydrate salt phase change energy storage material that eliminates the supercooling phenomenon prepared above is used to measure the supercooling degree of the inorganic hydrate salt phase change energy storage material with a thermal constant analyzer; The thermal performa...
Embodiment 2
[0028] The preparation method of inorganic hydrated salt phase change energy storage material at 15°C is as follows:
[0029] Calculated by the weight of a total amount of 100g, get 75g calcium chloride hexahydrate as inorganic hydrated salt, 9g xanthan gum as adhesive, 8g expanded graphite as heat conduction agent, 6g boric acid as modifier, 2g nanoscale material ( BC 4 and SiB 6 ) as a nucleating agent, magnetically stirred in a constant temperature water bath at 55°C for 1.4 hours until completely melted, and the prepared inorganic hydrate salt phase change energy storage material was packaged and stored in a packaging machine for future use.
[0030] The inorganic hydrate salt phase change energy storage material that eliminates the supercooling phenomenon prepared above is used to measure the supercooling degree of the inorganic hydrate salt phase change energy storage material with a thermal constant analyzer; The thermal performance test measures the phase change temp...
Embodiment 3
[0032] The preparation method of inorganic hydrated salt phase change energy storage material at 25°C is as follows:
[0033] Calculated by the weight of a total of 100g, take 65g of calcium chloride hexahydrate as inorganic hydrated salt, 10g of xanthan gum as adhesive, 15g of expanded graphite as thermal conductivity agent, 8g of sodium hexametaphosphate as modifier, 2g of nano grade material (SiB 6 ) as a nucleating agent, magnetically stirred in a constant temperature water bath at 50°C for 1.5 hours until completely melted, and the prepared inorganic hydrate salt phase change energy storage material was packaged and stored in a packaging machine for future use.
[0034] The inorganic hydrate salt phase change energy storage material that eliminates the supercooling phenomenon prepared above is used to measure the supercooling degree of the inorganic hydrate salt phase change energy storage material with a thermal constant analyzer; The thermal performance test measures t...
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