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Production method of colloid emulsifying agent

A production method and technology of emulsifiers, applied in food ingredients as emulsifiers, food ingredients containing natural extracts, food science, etc., can solve complex problems

Inactive Publication Date: 2018-08-31
CHENGDU MO NI TA TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Most of the existing production methods are relatively complicated. Colloids are used as emulsifiers. The advantages and disadvantages of the production methods are of great economic significance for improving product quality and reducing by-product content.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0005] The production method of the colloidal emulsifier, the main steps are: the orange peel is crushed to an average diameter of 1.3mm, soaked in water for 50min, then boiled for 20min, and the orange peel after draining the water is 0.05mol / L hydrochloric acid with 13 times concentration, Soak and hydrolyze at 60°C for 3h, filter and clarify the hydrolyzate, concentrate, add activated carbon and decolorize at 70°C for 30min, add 900mL ethanol with a mass fraction of 83% to the filtrate, press filter for 30min, wash with cyclohexanone solution for 70min, xylene Recrystallize in the solution, vacuum dry, and pulverize to obtain the finished product, wherein the mass fraction of the cyclohexanone solution is 35%, and the mass fraction of the xylene solution is 65%.

[0006] product quality

[0007] gel degree

example 2

[0009] The production method of the colloidal emulsifier, the main steps are: the orange peel is crushed to an average diameter of 1.6mm, soaked in water for 70min, then boiled for 40min, and the orange peel after draining is 0.05mol / L hydrochloric acid with 13 times the concentration, Soak and hydrolyze at 63°C for 5h, filter and clarify the hydrolyzate, concentrate, add activated carbon and decolorize at 70°C for 40min, add 1000mL ethanol with a mass fraction of 83% to the filtrate, press filter for 40min, wash with cyclohexanone solution for 90min, xylene Recrystallize in the solution, vacuum dry, and pulverize to obtain the finished product, wherein the mass fraction of the cyclohexanone solution is 39%, and the mass fraction of the xylene solution is 67%.

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PUM

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Abstract

The invention relates to a production method of a colloid emulsifying agent. The production method is characterized by comprising the main steps of crushing orange peel until the average diameter is 1.3-1.6mm, performing soaking with water for 50-70min, then performing boiling over for 20-40min, soaking the drained orange peel in hydrochloric acid of which the weight is 13 times of that of the drained orange peel and of which the concentration is 0.05mol / L at 60-63 DEG C for hydrolysis for 3-5h, filtering hydrolysis liquor, performing clarification, performing concentration, adding activated carbon, performing decoloration at 70 DEG C for 30-40min, adding 900-1000mL of ethanol of which the mass percentage is 83% to the filtrate, performing pressure filtration for 30-40min, performing washing with a cyclohexanone solution for 70-90min, performing recrystallization in a xylene solution, performing vacuum drying, and performing crushing to obtain finished products.

Description

technical field [0001] The invention relates to a compound production method, in particular to a production method of a colloidal emulsifier. Background technique [0002] Colloids are widely used in the food industry, mainly as gelling agents, thickeners, emulsifiers and stabilizers. Most pectins are used as gelling agents in the production of jams, jellies and candies. High methoxyl pectin is often used as a gelling agent in products with high sugar content and low pH. Low methoxyl pectin can be used as a gelling agent in milk and fruit. Ideal gelling agent for desserts. In addition, pectin is also widely used in the fields of medicine, textile and paper making, microbiology and so on. Pectin is a natural additive extracted from plants, so it is relatively safe. Most of the existing production methods are relatively complicated. Colloids are used as emulsifiers. The pros and cons of the production methods have important economic significance for improving product qualit...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L29/10
CPCA23L29/10A23V2002/00A23V2200/222A23V2250/21
Inventor 李红
Owner CHENGDU MO NI TA TECH CO LTD