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Method for preparing CN thin film through ion beam deposition

A technology of ion beam deposition and thin film, which is applied in the direction of ion implantation plating, coating, metal material coating process, etc., can solve the problem of difficult CN thin film, and achieve the effect of simple process and strong controllability

Inactive Publication Date: 2018-10-12
(CNBM) BENGBU DESIGN & RES INST FOR GLASS IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the traditional methods for preparing CN thin films all use N 2 as N source, since N 2 strong stability, it is difficult to make N 2 ionized and reacted with C to give CN film

Method used

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Examples

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Comparison scheme
Effect test

Embodiment Construction

[0010] The invention provides a method for preparing a CN thin film by ion beam deposition, comprising the following steps:

[0011] S1. Clean the substrate to remove oil and impurities on the surface of the substrate; ultra-clear high-transparency glass can be used as the substrate, and other conventional materials can also be used for the substrate;

[0012] S2. Adopt connected ion beam deposition equipment and ion implanter. The ion beam deposition equipment uses C target, and the C target is graphite with a purity of 99.99%. The substrate is placed in the vacuum chamber of the ion beam deposition equipment, and the vacuum degree reaches 1.0* 10 -3 At Pa, bombard the C target with argon ions, excite the C ions to sputter out, and pre-sputter the C target for 5 to 10 minutes to achieve the purpose of activating the target and removing the oxide on the target surface; then turn on the ion implanter at the same time and inject N ions, the implanted N ions react with the sputt...

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Abstract

The invention discloses a method for preparing a CN thin film through ion beam deposition. The method comprises following steps that S1, a substrate is cleaned, and oil contamination and impurities onthe surface of the substrate are removed; S2, an ion beam deposition device and an ion implantation machine which communicate are adopted, the ion beam deposition device adopts a target C, the substrate is placed in a vacuum cavity of the ion beam deposition device, argon ions are used for bombarding the target C, meanwhile, the ion implantation machine is started for injecting N ions, and the CNthin film is obtained from the surface of the substrate; the process parameters of the target C are independently controlled through the ion beam deposition device, providing of N ion sources is finished through the ion implantation machine, in the whole process, the ion beam deposition device and the ion implantation machine independently work and do not interfere with each other; C and N have asimple reaction to obtain the CN thin film, other ions do not exist, the process is simple, and controllability is higher.

Description

technical field [0001] The invention relates to the technical field of functional thin films, in particular to a method for preparing CN thin films by ion beam deposition. Background technique [0002] In the 1990s, some scientists predicted for the first time that CN, a compound that does not exist in nature, can be artificially synthesized, which has great polymerization energy and mechanical stability. Then Teter et al. speculated on the structure of CN and found that there are five kinds of CN compounds in the form of α phase, β phase, cubic phase, quasi-cubic phase and graphite-like phase. Studies have shown that except for the graphite-like phase, the theoretical values ​​of the bulk elastic modulus of the other four CNs can be compared with those of diamond, and are considered to be a new type of superhard material. At the same time, through the change of process performance, CN can have very high Very good physical and optical properties such as high resistivity and...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C14/46C23C14/48C23C14/06
CPCC23C14/0658C23C14/46C23C14/48
Inventor 沈洪雪倪嘉姚婷婷杨勇李刚
Owner (CNBM) BENGBU DESIGN & RES INST FOR GLASS IND CO LTD
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