Experimental device for improving yield of nano-particles prepared by metal wire electrical explosion

A nanoparticle and experimental device technology, applied in nanotechnology and other directions, can solve the problems of increasing production investment time and equipment costs, restricting the production and generation efficiency of nanoparticles, inconvenient operation and use, etc. The effect of energy utilization and reduction in the scale of production equipment

Inactive Publication Date: 2018-10-19
XI AN JIAOTONG UNIV
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  • Summary
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  • Description
  • Claims
  • Application Information

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Problems solved by technology

In recent years, the development of metal nanoparticle manufacturing technology has been very rapid, and a variety of nanopowder preparation methods have been designed, including gas condensation method, arc method, chemical reduction, and wire electric explosion. There are low production efficiency, there are not many devices that can realize the mass production of metal nanoparticles, and there are disadvantages such as complex structure, inconvenient operation and use, etc.
Metal nanoparticles can be prepared by using a metal wire to form an electric explosion process through a large current, but due to the influence of the energy efficiency of the electric explosion deposition and the inhomogeneity that occurs during the wire explosion process, the current electric explosion process generally occurs when the metal wire is thinner (<0.5mm ), the length is shorter (<200mm), which seriously restricts the output and generation efficiency of nanoparticles, and increases the time and equipment cost of production input.

Method used

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  • Experimental device for improving yield of nano-particles prepared by metal wire electrical explosion
  • Experimental device for improving yield of nano-particles prepared by metal wire electrical explosion
  • Experimental device for improving yield of nano-particles prepared by metal wire electrical explosion

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Embodiment 1

[0043] Nanoparticles of metal aluminum and copper have important application value in many fields due to their high specific surface area, high oxidation energy release rate, quantum size effect, high thermal conductivity, low resistance and efficient catalytic activity.

[0044] In the process of preparing nanoparticles by electric explosion of aluminum or copper wire, the inert gas argon is generally used as the protective gas, and the pressure is between 1.0 and 3.0 bar. An electric explosion occurs.

[0045] The capacity of the high-voltage pulse capacitor 11 is between 0.1-10.0 μF, the voltage is between 10-50 kV, and the electric explosion of a single aluminum wire is formed by the current pulse drive with a pulse of microsecond level by discharge. In order to increase the unit yield of nanoparticles, the device of the present invention can be used to improve the efficiency of electric explosion of metal wire, appropriately increase the capacitance, and adjust the curren...

Embodiment 2

[0048] During the preparation of metal aluminum and copper nanoparticles, the metal wire needs to be vaporized at a certain heating rate, which makes the explosion process of the metal wire often appear in the later stage of the rapid rise of the current, and then the energy stored in the pulse capacitor is very important for the formation of more nano particles. Particles are not contributing.

[0049] In order to improve the output of nanoparticles, the device of the present invention can be used to improve the electric explosion efficiency of the metal wire. After the first metal wire explodes, the energy in the pulse capacitor is transferred to the second metal wire, and the length of the second metal wire is adjusted so that The parameters of the electric explosion process are the same as those of the first metal wire. According to the length of the first metal wire, the length of the second metal wire can be 0.6-0.9 times the length of the first metal wire. This can ensu...

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Abstract

The invention discloses an experimental device for improving the yield of nano-particles prepared by metal wire electrical explosion. The device comprises a metal wire electric explosion test unit anda high-voltage pulse capacitor, one end of the high-voltage pulse capacitor is connected with a metal wire electric explosion test unit through a capacitor discharge switch, and the other end of thehigh-voltage pulse capacitor is in common connection with a metal cavity of the metal wire electric explosion test unit; and the metal wire electric explosion test unit comprises two sections of metalwires, the two-section metal wires are used for sequentially forming two electric explosion processes according to a discharge sequence in one pulse discharge process, and then the nano-particles arecorrespondingly generated. According to the device, double-wire electric explosion can be realized in a same experiment cavity, so that the size of the electric explosion experiment device can be greatly reduced, the volume of the experimental device is effectively reduced, and the production efficiency of the experimental device can be improved by 1.2-1.7 times.

Description

technical field [0001] The invention belongs to the technical field of preparing nanoparticles by electric explosion, and in particular relates to an experimental device for increasing the yield of nanoparticles prepared by electric explosion of metal wires in large-scale manufacturing of metal nano-parts. Background technique [0002] Metal nanoparticles have small size, large specific surface area, and quantum size effect. They have shown attractive application prospects in the fields of light absorption, sensitivity, catalysis, energy, and other functional materials, and have received widespread attention. In recent years, the development of metal nanoparticle manufacturing technology has been very rapid, and a variety of nanopowder preparation methods have been designed, including gas condensation method, arc method, chemical reduction, and wire electric explosion. There are low production efficiency, there are not many devices that can realize the mass production of met...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F9/14B82Y40/00
Inventor 陈立吴坚李兴文石恒通李鹏辉杨莉李梅
Owner XI AN JIAOTONG UNIV
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