Determination method for radix curcumae fingerprint and standard fingerprint thereof
A fingerprint and detection method technology, applied in the field of traditional Chinese medicine fingerprint analysis, can solve problems such as the inability to accurately express the volatile components of turmeric, extend the research on special requirements of varieties, etc., and achieve the effect of improving the quality control technology of medicinal materials
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0064] Example 1
[0065] 1. Instruments and reagents
[0066] 1.1 Instrument
[0067] One hundred thousandth electronic balance (METTLER TOLEDO), Agilent 7890A gas chromatograph, Waters liquid chromatograph. DB-624 column (30m*0.25mm*1.40μm), Phenomenex Gemini-NX C18 column (4.6×150mm, 5μm)
[0068] 1.2 Reagents
[0069] β-elemene reference substance, turmeric dione reference substance, n-hexane, ethanol, methanol
[0070] 2. Preparation of test product
[0071] Preparation of gas phase test solution: take 1.5g of turmeric medicinal material, put it in a 1000ml flask, add 100ml of water and count zeolite, and measure according to the volatile oil determination method. Add water from the upper end of the tester to fill the scale and overflow into the flask. 2ml n-hexane, connect to the reflux device, heat to boiling and keep slightly boiling for 3 hours, let cool, divide the n-hexane layer, put it in a 2ml measuring flask, wash the volatile oil extractor with a small amount of n-hexane,...
Example Embodiment
[0085] Example 2
[0086] 1. Instruments and reagents
[0087] 1.1 Instrument
[0088] One hundred thousandth electronic balance (METTLER TOLEDO), Agilent 7890A gas chromatograph, Waters liquid chromatograph. TraceGOLD TG-624 column (30m*0.25mm*1.40μm), Phenomenex Gemini-NX C18 column (4.6×150mm, 5μm)
[0089] 1.2 Reagents
[0090] β-elemene reference substance, turmeric dione reference substance, n-hexane, ethanol, methanol
[0091] 2. Preparation of test product
[0092] Preparation of gas phase test solution: take 1.5g of turmeric medicinal material, put it in a 1000ml flask, add 100ml of water and count zeolite, and measure according to the volatile oil determination method. Add water from the upper end of the tester to fill the scale and overflow into the flask. 2ml n-hexane, connect to the reflux device, heat to boiling and keep slightly boiling for 3 hours, let cool, divide the n-hexane layer, put it in a 2ml measuring flask, wash the volatile oil extractor with a small amount of...
Example Embodiment
[0107] Example 3
[0108] 1. Instruments and reagents
[0109] 1.1 Instrument
[0110] One hundred thousandth electronic balance (METTLER TOLEDO), Agilent 7890A gas chromatograph, Waters liquid chromatograph. OV-1301 column (30m*0.25mm*1.40μm), Agilent Eclipse XDB-C18 column (4.6×150mm, 5μm)
[0111] 1.2 Reagents
[0112] β-elemene reference substance, turmeric dione reference substance, n-hexane, ethanol, methanol
[0113] 2. Preparation of test product
[0114] Preparation of gas phase test solution: take 1.5g of turmeric medicinal material, put it in a 1000ml flask, add 100ml of water and count zeolite, and measure according to the volatile oil determination method. Add water from the upper end of the tester to fill the scale and overflow into the flask. 2ml n-hexane, connect to the reflux device, heat to boiling and keep slightly boiling for 3 hours, let cool, divide the n-hexane layer, put it in a 2ml measuring flask, wash the volatile oil extractor with a small amount of n-hexane,...
PUM
Property | Measurement | Unit |
---|---|---|
Column length | aaaaa | aaaaa |
The inside diameter of | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap