High-safety and storage-resistant stink composition
A composition and safety technology, applied in the direction of pest control, pest repellent, animal repellent, etc., to achieve the effect of toxicity and chemical hazard suppression and high safety
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Embodiment 1
[0028] A safe storage-resistant odor composition, the preparation method of the odor composition comprises the following steps:
[0029] (1) According to the mass ratio, weigh 25g of 85wt% phosphoric acid and add it into the dispersion kettle, then add 50g of distilled water and 12.7g of pseudo-boehmite into the dispersion kettle, mix and stir evenly to obtain mixture A, and add 65g of hydroxyl Tetra-n-butylamine aqueous solution was added to the reactor, and 3.1g of light silica was added to the reactor, and after stirring evenly, the mixture A was added to the reactor, and then 4.5g of di-n-propylamine was added to the reactor and 9.7g of Rh-Mo-S ternary compound, seal the reaction vessel, conduct crystallization treatment at a temperature of 195°C for 24 hours, and filter the product to obtain a solid after the crystallization treatment is completed;
[0030] (2) Repeatedly wash the solid matter in the above step twice with deionized water until the washed product is neutra...
Embodiment 2
[0038] A safe storage-resistant odor composition, the preparation method of the odor composition comprises the following steps:
[0039] (1) According to the mass ratio, weigh 25g of 85wt% phosphoric acid and add it into the dispersion kettle, then add 50g of distilled water and 12.7g of pseudo-boehmite into the dispersion kettle, mix and stir evenly to obtain mixture A, and add 65g of hydroxyl Tetra-n-butylamine aqueous solution was added to the reactor, and 3.1g of light silica was added to the reactor, and after stirring evenly, the mixture A was added to the reactor, and then 4.5g of di-n-propylamine was added to the reactor and 9.7g of the Rh-Se-S ternary compound, seal the reaction vessel, conduct crystallization treatment at a temperature of 205°C for 28 hours, and filter the product to obtain a solid after the crystallization treatment is completed;
[0040] (2) Repeatedly wash the solid matter in the above step 4 times with deionized water until the washed product is ne...
Embodiment 3
[0048] A safe storage-resistant odor composition, the preparation method of the odor composition comprises the following steps:
[0049] (1) According to the mass ratio, weigh 25g of 85wt% phosphoric acid and add it into the dispersion kettle, then add 50g of distilled water and 12.7g of pseudo-boehmite into the dispersion kettle, mix and stir evenly to obtain mixture A, and add 65g of hydroxyl Tetra-n-butylamine aqueous solution was added to the reactor, and 3.1g of light silica was added to the reactor, and after stirring evenly, the mixture A was added to the reactor, and then 4.5g of di-n-propylamine was added to the reactor and 9.7g of Rh-Mo-S ternary compound, seal the reaction vessel, conduct crystallization treatment at a temperature of 200°C for 26 hours, and filter the product to obtain a solid after the crystallization treatment is completed;
[0050] (2) Repeatedly wash the solid matter in the above step 3 times with deionized water until the washed product is neut...
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