Determining device of chloride ion diffusion coefficient in hydrated calcium silicate gel and determining method

A technology of calcium silicate hydrate and chloride ion diffusion, which can be used in measurement devices, diffusion analysis, instruments, etc., can solve the problem of inability to accurately measure the chloride ion diffusion coefficient of calcium silicate hydrate gel, and achieve good economical results. Benefit, simple and reasonable structure, short assembly time

Active Publication Date: 2018-12-11
HOHAI UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Technical problem to be solved: the existing measurement technology is only suitable for measuring the chloride ion diffusion coefficient of concrete whose main diffusion path is capillary pores, and cannot accurately measure the chloride ion diffusion coefficient of calcium silicate hydrate gel, and the chloride ion in water The main diffusion path in calcium silicate hydrate gel is gel hole, so the present invention proposes a measuring device and measuring method of chloride ion diffusion coefficient of calcium silicate hydrate gel, the device has the advantages of simple and reasonable structure, flexible application Good performance, low economic cost, simple and convenient operation, etc., the assay method is accurate and effective, and can quickly obtain the diffusion coefficient of chloride ions in calcium silicate hydrate gel

Method used

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  • Determining device of chloride ion diffusion coefficient in hydrated calcium silicate gel and determining method
  • Determining device of chloride ion diffusion coefficient in hydrated calcium silicate gel and determining method
  • Determining device of chloride ion diffusion coefficient in hydrated calcium silicate gel and determining method

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Embodiment 1

[0038] A measuring device for the chloride ion diffusion coefficient of hydrated calcium silicate gel, see figure 1 The measuring device includes a tank to be tested, a straight tube 3, a DC stabilized power supply 4, an elbow tube 5, a copper rod electrode 6, an anode test piece groove 7 and a cathode test piece groove 8. The elbow pipe 5 is set in the straight pipe 3 on both sides, and the elbow 5 and the straight pipe 3 are seamlessly connected, the groove to be tested is set in the middle of the inner side of the straight pipe 3, and the copper rod electrode 6 is respectively connected with the positive and negative electrodes of the DC stabilized power supply 4, and The copper rod electrodes 6 are respectively arranged in the pipe on one side of the tank to be tested and the pipe on the other side of the tank to be tested in the straight pipe 3, and the anode specimen tank 7 is where the copper rod electrode of the DC stabilized power supply 4 is connected with the positive ...

Embodiment 2

[0057] A measuring device for the chloride ion diffusion coefficient of hydrated calcium silicate gel, see figure 1 The measuring device includes a tank to be tested, a straight tube 3, a DC stabilized power supply 4, an elbow tube 5, a copper rod electrode 6, an anode test piece groove 7 and a cathode test piece groove 8. The elbow pipe 5 is set in the straight pipe 3 on both sides, and the elbow 5 and the straight pipe 3 are seamlessly connected, the groove to be tested is set in the middle of the inner side of the straight pipe 3, the copper rod electrode 6 is connected to the positive and negative electrodes of the DC stabilized power supply 4, and The copper rod electrodes 6 are respectively arranged in the pipe on one side of the tank to be tested and the pipe on the other side of the tank to be tested in the straight pipe 3. The anode specimen tank 7 is where the copper rod electrode of the DC stabilized power supply 4 is connected Inside the pipeline, the cathode sample ...

Embodiment 3

[0076] A measuring device for the chloride ion diffusion coefficient of hydrated calcium silicate gel, see figure 1 The measuring device includes a tank to be tested, a straight tube 3, a DC stabilized power supply 4, an elbow tube 5, a copper rod electrode 6, an anode test piece groove 7 and a cathode test piece groove 8. The elbow pipe 5 is set in the straight pipe 3 on both sides, and the elbow 5 and the straight pipe 3 are seamlessly connected, the groove to be tested is set in the middle of the inner side of the straight pipe 3, the copper rod electrode 6 is connected to the positive and negative electrodes of the DC stabilized power supply 4, and The copper rod electrodes 6 are respectively arranged in one side of the pipeline and the other side of the pipeline to be tested in the straight pipe 3, and the anode sample tank 7 is the inside of the pipeline where the copper rod electrode of the DC stabilized power supply 4 is connected with the positive electrode. The cathode...

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Abstract

The invention discloses a determining device of chloride ion diffusion coefficient in a hydrated calcium silicate gel and a determining method, which belongs to the technical field of determining thedurability of concrete structures. The determining device comprises a tank to be tested, a straight tube, a DC (direct current) stabilized power supply, an elbow, a copper rod electrode, an anode testpiece tank and a cathode test piece tank, and the determining method comprises preparation of a test piece to be detected, connection of the determining device, electromigration test and test resultprocessing. The determining method provides a method for preparing a test piece for changing a diffusion path of chloride ions from capillary pores to gel pores, wherein the capillary pores on the surface of the test piece prepared by the method are filled with epoxy resin, the internal capillary pores are in a dry state, and the gel pores of hydrated calcium silicate are in a wet state, so that the chloride ions have wet hydrated calcium silicate gel pores as a main diffusion path during test. The test device disclosed by the invention has a simple and reasonable structure and convenient operation, and can accurately obtain the diffusion coefficient of the chloride ions in the hydrated calcium silicate gel.

Description

Technical field [0001] The invention relates to a measuring device and a measuring method for the chloride ion diffusion coefficient of hydrated calcium silicate gel, and belongs to the technical field of concrete structure durability measurement. Background technique [0002] In coastal areas and cold areas (using deicing salt), the corrosion of steel bars caused by chloride ions is the main reason for the deterioration of the durability of concrete structures. The corrosion of steel bars has caused huge economic losses. Therefore, the resistance of concrete to chloride ion penetration has become an evaluation One of the important indicators of concrete durability. [0003] On the macro scale, concrete can be regarded as the interface transition zone, cement hydrate and aggregate. Among them, the cement hydrate mainly includes hydrated calcium silicate (C-S-H), calcium hydroxide crystal (CH) and sulfate salt. In the past few decades, scholars from all over the world have done a l...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N13/00
CPCG01N13/00G01N2013/003
Inventor 刘琳陶广慧宋丹雅徐夏佺
Owner HOHAI UNIV
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