Fiber composite material for robotic electronic skin and preparation method thereof
A fiber composite material and electronic skin technology, which is applied in fiber type, fiber treatment, hollow filament manufacturing, etc., can solve the problems of low sensitivity, poor mechanical properties of pure liquid metal, weak tensile properties and electrical conductivity, etc. problems, to achieve the effect of excellent conductivity, broad application prospects, and good stretchability
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Embodiment 1
[0029] a. Add pyromellitic dianhydride and 4,4'-diphenyl ether diamine into N-methylpyrrolidone, and obtain polyamic acid solution through polycondensation reaction. The temperature of polycondensation reaction is 8°C, and the time is 4h. Wet spinning and thermal stretching, the temperature of thermal stretching is 290°C, and the stretching ratio is 2 times; hollow polyimide fibers are obtained; wherein, 12 parts by weight of pyromellitic dianhydride, 4,4' - 18 parts by weight of diphenyl ether diamine, 70 parts by weight of N-methylpyrrolidone;
[0030] b. Rinse the hollow polyimide fiber prepared in step a, and slowly immerse it in the tin-gallium liquid metal, in the tin-gallium liquid metal, 45 parts by weight of tin and 55 parts by weight of gallium; take it out after standing at 70°C for 25 minutes, And repeat the immersion and removal, the number of repetitions is 4 times; the tin-gallium liquid metal is filled with the hollow polyimide fiber;
[0031] c. Place the hol...
Embodiment 2
[0033] a. Add pyromellitic dianhydride and 4,4'-diphenyl ether diamine into N-methylpyrrolidone, and obtain polyamic acid solution through polycondensation reaction. The temperature of polycondensation reaction is 8°C, and the time is 3.5h. After wet spinning and thermal stretching, the temperature of thermal stretching is 295°C, and the draw ratio is 3 times; hollow polyimide fibers are obtained; wherein, 14 parts by weight of pyromellitic dianhydride, 4,4 19 parts by weight of '-diphenyl ether diamine, 67 parts by weight of N-methylpyrrolidone;
[0034] b. Rinse the hollow polyimide fiber prepared in step a, and slowly immerse it in the tin-gallium liquid metal, in the tin-gallium liquid metal, 50 parts by weight of tin and 50 parts by weight of gallium; take it out after standing at 80° C. for 27 minutes, And repeat the immersion and removal, the number of repetitions is 5 times; make the tin-gallium liquid metal fill the hollow polyimide fiber;
[0035] c. Place the hollo...
Embodiment 3
[0037] a. Add pyromellitic dianhydride and 4,4'-diphenyl ether diamine into N-methylpyrrolidone, and obtain polyamic acid solution through polycondensation reaction. The temperature of polycondensation reaction is 10°C, and the time is 3h. Wet spinning and thermal stretching, the temperature of thermal stretching is 300°C, and the stretching ratio is 3 times; hollow polyimide fibers are obtained; wherein, 15 parts by weight of pyromellitic dianhydride, 4,4' - 20 parts by weight of diphenyl ether diamine, 65 parts by weight of N-methylpyrrolidone;
[0038] b. Rinse the hollow polyimide fiber prepared in step a, and slowly immerse it in the tin-gallium liquid metal, in the tin-gallium liquid metal, 60 parts by weight of tin and 40 parts by weight of gallium; take it out after standing at 80° C. for 30 minutes, And repeat the immersion and removal, the number of repetitions is 5 times; make the tin-gallium liquid metal fill the hollow polyimide fiber;
[0039]c. Place the hollow...
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