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Etherification catalytic distillation module

A catalytic rectification and etherification technology, which is applied in distillation separation, chemical instruments and methods, chemical/physical processes, etc., can solve the problem of unfavorable mass transfer between gas-liquid two-phase, unfavorable gas-liquid mass transfer, and affecting tower separation Effect and other issues, to achieve the effect of improved catalytic reaction efficiency, low energy consumption, and stable catalytic effect

Pending Publication Date: 2019-04-09
丹东明珠特种树脂有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are also many technical problems in that the gas-liquid two phases pass through their respective channels in the reaction section, and the mass transfer between the gas-liquid two phases is not easy to occur. When the flow is upward, the liquid flows downward along the surface of the packing sheet to form a liquid film, and most of it flows downward along the surface of the trough. The liquid film at the trough is thicker but the peak is in a naked state, which makes the liquid distribution in the tower uneven; in addition, the liquid at the trough After the membrane is formed, the liquid channel in the tower will remain basically unchanged for a long time, which is not conducive to the mass transfer between gas and liquid and affects the separation effect of the tower
Therefore, this prior art is not suitable for use in a gas-liquid-solid three-phase system in which both gas and liquid are reaction materials

Method used

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  • Etherification catalytic distillation module
  • Etherification catalytic distillation module
  • Etherification catalytic distillation module

Examples

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Embodiment 1

[0021] The etherification catalytic rectification module of the present application is applied in a catalytic rectification tower preparation device for producing methyl tert-butyl by C4 catalytic rectification. The diameter of the catalytic rectification tower used is 2400mm, including 19 trays in the rectification section; 10 reaction sections are installed in the catalytic rectification tower, and each reaction section is filled with a 1600mm high etherification catalytic rectification module. A liquid redistributor is installed between them; under the reaction section is the stripping section, with a total of 39 trays; the catalyst used in this etherification catalytic rectification module is the D005-II resin catalyst of Dandong Mingzhu Special Resin Co., Ltd.

Embodiment 2

[0027] The etherification catalytic rectification module of this patent application is applied to the catalytic rectification tower industrial device for producing methyl tert-amyl ether from isopentene. The diameter of the catalytic rectification tower device is 2400mm, and there are 19 trays in the rectification section; the catalytic rectification The tower is filled with 10 reaction sections, and each reaction section is filled with etherification catalytic rectification modules with a height of 1600mm, and liquid redistributors are installed between the etherification catalytic rectification modules; under the reaction section is the stripping section with a total of 39 trays; The catalyst used in the etherification catalytic rectification module is the D005-IIs resin catalyst of Dandong Mingzhu Special Resin Co., Ltd.

Embodiment 3

[0033] The etherification catalytic rectification module of this patent application is applied to the light gasoline etherification catalytic rectification tower industrial device. The diameter of the catalytic rectification tower is 2400mm, including 19 trays in the rectification section; 10 reaction sections are installed in the catalytic rectification tower, and each reaction section is filled with a 1600mm high etherification catalytic rectification module. A liquid redistributor is installed between them; under the reaction section is the stripping section with a total of 39 trays; the catalyst used in the etherification catalytic rectification module is the D005-IIs resin catalyst of Dandong Mingzhu Special Resin Co., Ltd.

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Abstract

The application provides an etherification catalytic distillation module formed by staggering and arranging a catalyst layer and a stainless steel corrugated plate group; the catalyst layer comprisescatalyst particles, packing sheets and a stainless steel mesh, wherein the packing sheets are at least two parallel stainless steel corrugated plates, a gap space of the stainless steel corrugated plates is filled with the catalyst particles, and then, the catalyst particles are wrapped by the stainless steel mesh; and the stainless steel corrugated plates are provided with a plurality of diversion windows at wave peaks and wave troughs. By adopting the technical scheme, the liquid-phase surface updating and the radial distribution uniformity are effectively promoted, the gas-liquid mass transfer is further improved, and the etherification catalytic distillation module has the technical advantages of easily controlled reaction section bed layer temperature, temperature runaway avoidance, higher operation flexibility, wide operation load, convenience in assembly and disassembly, stable catalyst effect, little catalyst wear, no catalyst leakage and simplicity in industrial application.

Description

technical field [0001] This patent application relates to a chemical reaction device, in particular to a catalytic rectification packing component for a chemical catalytic rectification reaction. Background technique [0002] Catalytic rectification organically couples catalytic reaction and rectification operation. The catalytic reaction is carried out in the reaction section of the catalytic rectification tower, and rectification separation is carried out at the same time to separate the product from the reactant and push the equilibrium reaction to move to the right, achieving good results. High conversion rate, selectivity and product purity, and achieve the technical purpose of reducing energy consumption. Catalytic distillation technology is widely used in chemical manufacturing fields such as etherification, isomerization, selective hydrogenation, and alkylation. The technical core of catalytic rectification is the modular structure of catalytic rectification, and ma...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/02B01D3/00
CPCB01D3/009B01J8/008B01J8/0242
Inventor 吕晓东陈晓光周洪涛宋寿康赵旺华徐振涛王晋薛英明郑英杰杨松
Owner 丹东明珠特种树脂有限公司
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