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High-temperature high-grade magnesia porcelain preparation method

A magnesia porcelain, high-grade technology, applied in the field of high-temperature and high-grade magnesia porcelain preparation, can solve the problems of narrow firing temperature range, easy generation of pinhole defects, difficult temperature control, etc., to eliminate glaze pinholes and eliminate residual Stress, the effect of improving glaze brightness

Inactive Publication Date: 2019-06-25
叶剑
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, most of the domestic high-temperature magnesia porcelain preparation methods adopt a one-time firing process, but due to the narrow firing temperature range of magnesia porcelain, it is difficult to control the temperature during the firing process. When the temperature is too high or the holding time is too long, it is easy to produce deformation defects. When the temperature is too low or the holding time is short, cracking defects are easy to occur. Therefore, in the production process of medium-temperature magnesia porcelain, about 30% raw talc is often added in order to widen the firing range. However, due to the one-time firing process, its During the firing process, more pinhole defects will be produced on the glaze surface due to the decomposition of raw talc. In addition, due to the large expansion coefficient of the magnesia porcelain body, the expansion coefficient of the glaze must match it, and the glossiness of the glaze surface after one firing Poor and easy to produce pinhole defects, so the current preparation methods of high-temperature magnesia porcelain can no longer meet the needs of consumers, which seriously hinders the improvement of the quality of high-temperature magnesia daily-use ceramics

Method used

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Embodiment 1

[0013] Implementation column one:

[0014] A method for preparing high-temperature high-grade magnesia porcelain. The raw material is weighed according to mass percentage: 41% burnt talc, 21% raw talc, 10% feldspar, 11% kaolin, 3% bentonite, and 14% quartz. The fineness of the milled mud is 0.008% and the sieve with more than 10,000 holes. After the mud is stale, the green body is obtained by grouting. The green body has been bisque-fired in advance. The biscuit firing temperature is 1280 ° C and the holding time is 30 minutes;

[0015] Weigh the glaze material according to the mass percentage: 33% feldspar, 15% calcite, 8% kaolin, 10% quartz, 4% ZnO, 30% glass frit, after mixed ball milling, the fineness of the grinding mud is controlled to be 0.03% per hole Sieve the remainder, then glaze the inner and outer surfaces of the plain-fired plain tire, dry it, and fire it at 1200°C for 30 minutes.

[0016] The prepared sample was tested for gloss performance, and the gloss was 8...

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Abstract

The invention relates to a high-temperature high-grade magnesia porcelain preparation method, wherein the billet material comprises, by weight, 30-45% of burned talc, 20-35% of raw talc, 5-15% of feldspar, 10-18% of kaolin, 3-5% of bentonite, and 0-15% of quartz, and the glaze material comprises, by weight, 20-40% of feldspar, 5-15% of calcite, 4-8% of kaolin, 0-15% of quartz, 3-5% of ZnO, 0-5% ofBaCO3, and 20-35% of frit. According to the preparation method, billet material and glaze material preparation, molding, drying, biscuit firing of billet body, glazing, drying, and medium temperatureglaze burning to obtain the product, wherein the biscuit firing temperature is 1280-1300 DEGC, the thermal insulation is 30 min, the medium temperature glaze burning temperature is 1200 DEGC, and thethermal insulation is 30 min. According to the present invention, with the preparation method, the product with advantages of good glaze surface quality and high glossiness is obtained so as to achieve broad application prospects.

Description

technical field [0001] The invention belongs to the field of inorganic non-metallic materials (ceramics), and specifically relates to a preparation method of high-temperature high-grade magnesia porcelain. Background technique [0002] At present, most domestic high-temperature magnesia porcelain preparation methods adopt a one-time firing process, but due to the narrow firing temperature range of magnesia porcelain, it is difficult to control the temperature during the firing process. When the temperature is too high or the holding time is too long, it is easy to produce deformation defects. When the temperature is too low or the holding time is short, cracking defects are easy to occur. Therefore, in the current production process of medium-temperature magnesia porcelain, in order to expand the firing range, about 30% raw talc is often added. However, due to the one-time firing process, its During the firing process, more pinhole defects will be produced on the glaze surfa...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/20C04B41/86C04B35/622C04B35/64C03C8/00
Inventor 叶剑
Owner 叶剑
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