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Method for dispersing solid particles in water

A solid particle, solid technology, applied in the field of fine chemical preparations, to solve the problem of rapid cooling and good stability

Active Publication Date: 2019-06-25
南京瑞思化学技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The present invention changes the previous process of dispersing solid particles in water, and the dispersant is adsorbed on the surface of solid particles by ball grinding, which solves the problem of rapid cooling and obtains a dispersion with better stability

Method used

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  • Method for dispersing solid particles in water

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] While maintaining the system temperature at 15°C, disperse 3 parts of stearyl alcohol, 3 parts of lauryl stearate, and 4 parts of 70# microcrystalline wax into particles with a diameter of less than 1mm in a high-speed pulverizer to obtain solid mixture I;

[0037] Add 5 parts of 68# white oil, 10 parts of the solid mixture I obtained above, 0.3 parts of secondary alcohol polyoxyethylene ether (30), 0.3 parts of sodium lauryl phosphate and 10 parts of water into the ball mill, and keep the rotation speed at 200rpm Stir to form a solid-liquid mixture II that can be stirred;

[0038] Add balls with a diameter of 0.6~1.0mm and 0.1 part of defoamer to the above solid-liquid mixture II, keep the system temperature at 30±2°C, increase the speed to 1000rpm, grind for 10min; then add 13.5 parts of water to the system, Make the solid content of the dispersion liquid 40%, add balls with a diameter of 0.3~0.6mm, and continue grinding for 100min;

[0039] Finally, add the remainin...

Embodiment 2

[0041] While maintaining the system temperature at 18°C, disperse 20 parts of behenyl alcohol, 3 parts of pentaerythritol stearate, and 3 parts of paraffin into particles with a diameter of less than 1 mm in a high-speed pulverizer to obtain solid mixture I;

[0042] Add 26 parts of the solid mixture I obtained above, 1 part of branched chain secondary alcohol polyoxyethylene ether (20), 0.8 part of Pingpingjia O-25, 1.2 parts of NNO, and 15 parts of water into the ball mill, and keep stirring at 450 rpm , forming a solid-liquid mixture II that can be stirred;

[0043] Add balls with a diameter of 0.6~1.0mm and 0.3 parts of defoamer to the above solid-liquid mixture II, keep the system temperature at 20±2°C, increase the speed to 3000rpm, and grind for 25 minutes; then add 13.7 parts of water to the system, Make the solid content of the dispersion liquid 50%, add balls with a diameter of 0.3~0.6mm, and continue grinding for 40 minutes;

[0044] Finally, add the remaining 41 p...

Embodiment 3

[0046]While maintaining the system temperature at 10°C, disperse 10 parts of lauryl alcohol, 9 parts of stearyl palmitate, and 3 parts of rubber protective wax into particles with a diameter of less than 1 mm in a high-speed pulverizer to obtain solid mixture I;

[0047] Add 6 parts of alkylbenzene, 22 parts of the solid mixture I obtained above, 1.2 parts of octylphenol polyoxyethylene ether (30), 0.8 parts of AES and 15 parts of water into the ball mill, and keep stirring at 100 rpm to form a stirring The solid-liquid mixture II;

[0048] Add balls with a diameter of 0.6~1.0mm and 0.5 parts of defoamer to the above solid-liquid mixture II, keep the system temperature at 35±2°C, increase the speed to 5000rpm, and grind for 30 minutes; then add 14.5 parts of water to the system, Make the solid content of the dispersion liquid 50%, add balls with a diameter of 0.3~0.6mm, and continue grinding for 20 minutes;

[0049] Finally, the remaining 39.8 parts of water were added to the...

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Abstract

The invention relates to a method for dispersing solid particles in water. A formed dispersion liquid comprises higher fatty alcohol, fatty acid ester, hydrocarbon substances, a dispersing agent, a defoaming agent, a thickening agent, water and the like. The dispersing agent is adsorbed on the surface of the solid particles through grinding of ball beads, so that a stable dispersion liquid is formed. According to the method, a high-temperature and rapid cooling process is not involved, the production energy consumption is greatly reduced, and the method can be used for producing a waterproof agent, a release agent, an isolating agent and a defoaming agent.

Description

technical field [0001] The invention relates to a method for dispersing solid particles in water, which can be used to manufacture wax emulsions and solid fatty alcohol emulsions, and belongs to the technical field of fine chemical preparations. Background technique [0002] The dispersion liquid formed by dispersing solid particles in water has many important fields in the national economy. For example, according to different uses, waxes with different melting points are dispersed in water to make waterproofing agent, release agent, and mold release agent; another example is the wet end of papermaking. The foam control agent in chemistry is also a degassing agent formed by dispersing higher fatty alcohols and waxes in water. Therefore, the technique of dispersing solid particles in water is an important technique. [0003] Many companies and scholars at home and abroad are also researching the preparation method of this dispersion: patent 201810515487.5 introduces the prep...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J3/05C08L91/06C08L23/06C08K5/05C08K5/101C08K5/103
Inventor 吴飞其他发明人请求不公开姓名
Owner 南京瑞思化学技术有限公司