Preparation method of dry process black silicon battery
A black silicon, battery technology, applied in circuits, electrical components, final product manufacturing, etc., can solve problems such as difficult to achieve
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Embodiment 1
[0030] (1), acid corrosion texturing
[0031] The ingredients used are HF: HNO 3 :H 2 A mixed solution of O=2:4:3 (volume ratio) is used for texturing diamond wire polysilicon wafers.
[0032] (2), RIE Texturing
[0033] Use volume ratio as SF 6 :0 2 :Cl 2 =8:10:5 mixed gas, the plasma etches the front surface of the textured silicon wafer to form a nano-textured surface, SF 6 The flow rate is 1600sccm, O 2 The flow rate is 2000sccm, Cl 2 The flow rate is 1000sccm, the pressure is 30 Pa, the speed is 18mm / s, the micro-nano opening width is controlled at 300-400mm, and the depth is at 150-190nm. Reflectivity 4-7%;
[0034] (3), cleaning after RIE
[0035] The ingredients used are BOE: H 2 o 2 :H 2 The mixed solution of O=1:2:3 (volume ratio) was used to optimize the texture of the silicon wafer after RIE, the reaction time was 7min, and the reaction temperature was 40°C. Then perform water washing-HF washing-water washing-HCl washing-water washing in order to remo...
Embodiment 2
[0046] (1), acid corrosion texturing
[0047] The ingredients used are HF: HNO 3 :H 2 A mixed solution of O=2:4:3 (volume ratio) is used for texturing diamond wire polysilicon wafers.
[0048] (2), RIE Texturing
[0049] Use volume ratio as SF 6 :0 2 :Cl 2 =8:10:5 mixed gas, the plasma etches the front surface of the textured silicon wafer to form a nano-textured surface, SF 6 The flow rate is 1120sccm, O 2The flow rate is 1400sccm, Cl 2 The flow rate is 700sccm, the pressure is 25 Pa, the speed is 10mm / s, the micro-nano opening width is controlled at 300-400mm, and the depth is at 150-190nm. Reflectivity 4-7%;
[0050] (3), cleaning after RIE
[0051] The ingredients used are BOE: H 2 o 2 :H 2 The mixed solution of O=1:2:3 (volume ratio) was used to optimize the texture of the silicon wafer after RIE, the reaction time was 6 minutes, and the reaction temperature was 40°C. Then perform water washing-HF washing-water washing-HCl washing-water washing in order to r...
Embodiment 3
[0062] (1), acid corrosion texturing
[0063] The ingredients used are HF: HNO 3 :H 2 A mixed solution of O=2:4:3 (volume ratio) is used for texturing diamond wire polysilicon wafers.
[0064] (2), RIE Texturing
[0065] Use volume ratio as SF 6 :0 2 :Cl 2 =8:10:5 (volume ratio) mixed gas, plasma etches the positive surface of the silicon wafer after texturing to form nano-texture, SF 6 The flow rate is 1600sccm, O 2 The flow rate is 2000sccm, Cl 2 The flow rate is 1000sccm, the pressure is 30 Pa, the speed is 18mm / s, the micro-nano opening width is controlled at 300-400mm, and the depth is at 150-190nm. Reflectivity 4-7%;
[0066] (3), cleaning after RIE
[0067] The ingredients used are BOE: H 2 o 2 :H 2 The mixed solution of O=1:2:3 (volume ratio) was used to optimize the texture of the silicon wafer after RIE, the reaction time was 8min, and the reaction temperature was 40°C. Then perform water washing-HF washing-water washing-HCl washing-water washing in ord...
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