A sample preparation method for observing the crystallographic orientation of the inner grains of the Al metallization of an igbt chip
A technology for sample preparation and metallization, which is used in the preparation of test samples, material analysis using wave/particle radiation, sampling, etc. Problems such as observation of metallization layer
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[0034] A method for preparing a sample for observing the grain direction in the Al metallization of an IGBT chip, characterized in that it comprises the following steps:
[0035] A) Remove the outer package of the high-power IGBT module by machining;
[0036] B) Set the temperature of the constant-temperature heating platform to 250°C, place the high-power IGBT module on the constant-temperature heating platform, and keep the bottom plate of the power module in contact with the constant-temperature heating platform for about 30 seconds, until the solder layer between the copper-clad ceramic substrate and the bottom plate is melted, Remove the bottom plate of the module, and the module structure at this time only leaves the high-power IGBT chip layer and the copper-clad ceramic substrate;
[0037] C) soaking the remaining structure of the high-power IGBT module in step B) in a silica gel remover for 12 hours to remove the silica gel on the surface of the IGBT chip;
[0038] D)...
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