Chloride-free alkali-free liquid setting accelerator and preparation method thereof
A technology of liquid accelerator and stabilizer, applied in the field of chlorine-free and alkali-free liquid accelerator and its preparation, can solve the problems of strong corrosion, large loss of concrete strength, long shelf life, etc. Small, the effect of increasing the coagulation speed
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Embodiment 1
[0031] A preparation method of chlorine-free and alkali-free liquid quick-setting agent, comprising the following steps:
[0032] Step 1, preparation of aluminum fluorosilicate: add 48% fluorosilicic acid, 32% aluminum hydroxide (industrial first-grade product) and 20% tap water to the reactor, heat and stir at a temperature of 60°C and a speed of 400 rpm 1.5h, aluminum fluorosilicate was obtained.
[0033] Step 2: Mix 10% aluminum fluorosilicate with 30% water, stir and react for 40 minutes at a temperature of 60°C and a rotational speed of 400 rpm to completely dissolve the aluminum fluorosilicate to obtain an aluminum fluorosilicate solution.
[0034] Step 3: Add 50% aluminum sulfate octadecahydrate to the aluminum fluorosilicate solution, and continue stirring for 55 minutes at a temperature of 60°C and a rotation speed of 400 rpm to obtain a stirring solution.
[0035] Step 4, add 5% diethanol monoisopropanolamine, 1% dodecyl dimethyl amine oxide and the remaining water ...
Embodiment 2
[0037] A preparation method of chlorine-free and alkali-free liquid quick-setting agent, comprising the following steps:
[0038] Step 1, preparation of aluminum fluorosilicate: add 48% fluorosilicic acid, 32% aluminum hydroxide (industrial first-grade product) and 20% tap water to the reactor, heat and stir at a temperature of 60°C and a speed of 400 rpm 1h, aluminum fluorosilicate was obtained.
[0039] Step 2: Mix 20% aluminum fluorosilicate with 30% water, stir and react for 40 minutes at a temperature of 60°C and a rotational speed of 400 rpm to completely dissolve the aluminum fluorosilicate to obtain an aluminum fluorosilicate solution.
[0040] Step 3: Add 40% aluminum sulfate octadecahydrate to the aluminum fluorosilicate solution, and continue stirring for 55 minutes at a temperature of 60°C and a rotation speed of 400 rpm to obtain a stirring solution.
[0041] Step 4: Add 3% diethanol monoisopropanolamine, 1.5% dodecyl dimethyl amine oxide and the remaining water ...
Embodiment 3
[0043] A preparation method of chlorine-free and alkali-free liquid quick-setting agent, comprising the following steps:
[0044] Step 1, preparation of aluminum fluorosilicate: add 53% fluorosilicic acid, 37% aluminum hydroxide (industrial first-grade product) and 10% tap water into the reactor, heat and stir at a temperature of 60°C and a speed of 400 rpm 2h, in aluminum fluorosilicate.
[0045] Step 2: Mix 20% aluminum fluorosilicate with 30% water, stir and react for 40 minutes at a temperature of 60°C and a rotational speed of 400 rpm to completely dissolve the aluminum fluorosilicate to obtain an aluminum fluorosilicate solution.
[0046] Step 3: Add 40% aluminum sulfate octadecahydrate to the aluminum fluorosilicate solution, and continue stirring for 55 minutes at a temperature of 60°C and a rotation speed of 400 rpm to obtain a stirring solution.
[0047] Step 4, add 5% diethanol monoisopropanolamine, 1% dodecyl dimethyl amine oxide and the remaining water to the sti...
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