A kind of fingerprint detection method of Wenjing Decoction
A technology of fingerprint spectrum and detection method, which is applied in the detection field of medicinal preparations, can solve the problems of inability to reflect the overall characteristics of traditional Chinese medicine compound preparations, incomplete drug quality, etc., and achieve the effects of reducing artificial processing, good absorption value and stable baseline.
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[0096] 1. Preparation of Wenjingtang Standard Decoction Mixed Reference Substance Solution: Precisely weigh ferulic acid, paeoniflorin, cinnamon aldehyde, paeonol, gemaconone, ginsenoside Rg1, ginsenoside Re, ginsenoside Rb1, liquiritin , ammonium glycyrrhizinate, and β-ecdysterone reference substance, add methanol to make mixed reference substances with mass concentrations of 129.5, 89.2, 321.4, 58.7, 232.6, 117.9, 235.6, 124.8, 136.2, 259.3, 285.6 μg / mL solution;
[0097] 2. Preparation of Wenjing Decoction Standard Decoction Test Solution: Weigh 1.67g each of Angelica, Chuanxiong, Paeoniae Alba, Cinnamon, Cortex Moutan, and Curcuma powder, 3.33g each of Ginseng, Licorice, and Achyranthes bidentata powder, add 300mL of water, mix Mix evenly, first heat to boiling with strong fire, then switch to slow fire and fry slowly. When the decoction reaches about 160mL, filter it while it is hot, add water to the filtrate to 250mL, accurately absorb 10mL of standard decoction of Wenji...
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