Thermostable indoor set-off smokeless sulfur-free cold firework medicament and preparation method thereof

A heat-stabilized and firework-based technology, applied in the direction of non-explosive stabilizers, non-explosive/non-thermic components, explosives, etc., can solve problems such as smoke pollution, achieve full combustion, low discharge temperature, and fewer steps

Pending Publication Date: 2020-04-03
江西吉润花炮新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The present invention provides a heat-stable indoor discharge smokeless and sulfur-free cold smoke flower medicament and its pre

Method used

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  • Thermostable indoor set-off smokeless sulfur-free cold firework medicament and preparation method thereof
  • Thermostable indoor set-off smokeless sulfur-free cold firework medicament and preparation method thereof
  • Thermostable indoor set-off smokeless sulfur-free cold firework medicament and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] A heat-stable indoor discharge smokeless and sulfur-free cold fireworks agent, the mass percentage of each component is as follows:

[0027]

[0028] Take 23.47g of nitrobamboo cellulose powder and divide it into two groups, A and B, wherein 7.47g of group A and 16g of group B, and dissolve the nitrobamboo cellulose powder of group A in 74.7g of ethyl acetate, and stir under the condition of ultrasonic dispersion 2.3 hours, then continue under stirring state, add 5.59g polyethylene wax powder and 11.63g zinc stearate powder, stir well, make nitrocellulose mixed sol;

[0029] Add 40g of pentaerythritol tetranitrate powder and 2.96g of titanate coupling agent to 400g of acetone, and ultrasonically disperse for 42 minutes to obtain a mixed solution C; transfer the mixed solution C to an ice-water bath for stirring; then add 0.83g of polyethylene Add the alcohol butyral adhesive to the mixed solution C and stir for 3.7 hours; transfer the reaction device to an oil bath a...

Embodiment 2

[0036] A heat-stable indoor discharge smokeless and sulfur-free cold fireworks agent, the mass percentage of each component is as follows:

[0037]

[0038]

[0039] Take 6.82kg of nitrobamboo cellulose powder and divide it into two groups, A and B, wherein 1.82kg of group A and 5kg of group B, and dissolve the nitrobamboo cellulose powder of group A in 18.2kg of ethyl acetate, and stir under the condition of ultrasonic dispersion 2.7 hours, then continue under stirring state, add 1.29kg polyethylene wax powder and 2.09kg zinc stearate powder, stir, make nitrocellulose mixed sol;

[0040] Add 13kg of pentaerythritol tetranitrate powder and 0.91kg of titanate coupling agent to 130kg of acetone and disperse ultrasonically for 38 minutes to obtain mixed solution C; transfer mixed solution C to an ice-water bath for stirring; then add 0.28kg of polyethylene Add the alcohol butyral adhesive to the mixed solution C and stir for 4.2 hours; transfer the reaction device to an oil b...

Embodiment 3

[0047] A heat-stable indoor discharge smokeless and sulfur-free cold fireworks agent, the mass percentage of each component is as follows:

[0048]

[0049]

[0050] Take 26.13kg of nitrobamboo cellulose powder and divide it into two groups, A and B, wherein group A is 8.13kg and group B is 18kg, and the nitrocellulose powder of group A is dissolved in 81.3kg of ethyl acetate, and stirred under the condition of ultrasonic dispersion 2.3 hours, then continue under stirring state, add 6.28kg polyethylene wax powder and 16.55kg zinc stearate powder, stir evenly, make nitrocellulose mixed sol;

[0051] Add 66kg of pentaerythritol tetranitrate powder and 4.62kg of titanate coupling agent to 660kg of acetone, and ultrasonically disperse for 50 minutes to obtain a mixed solution C; transfer the mixed solution C to an ice-water bath for stirring; then add 1.34kg of polyethylene Add the alcohol butyral adhesive to the mixed solution C and stir for 3.5 hours; transfer the reaction...

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PUM

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Abstract

The invention relates to a thermostable indoor set-off smokeless sulfur-free cold firework medicament and a preparation method thereof, and belongs to the field of environment-friendly pyrotechnic compositions. The firework medicament is composed of the components: nano titanium-magnesium powder, modified pentaerythritol tetranitrate, zirconium deuteride, dihydroxy glyoxime, nitrobamboo cellulose,dimethyl diphenyl urea, zinc stearate, nitro tert-butyl triol trinitrate, polyethylene wax and diatomite. The nano magnesium-aluminum powder and the modified pentaerythritol tetranitrate powder are used as main components, so that the setting-off temperature is low, and safety and reliability are realized; dihydroxy glyoxime and zirconium deuteride are introduced, so that sufficient combustion and bright color are ensured; the components do not contain chlorine elements and sulfur elements, so that no toxic and harmful smoke is generated; self-made nitrated bamboo cellulose is adopted, and dimethyl diphenyl urea is introduced, so that the compatibility and the mechanical property of the cold firework medicament can be effectively improved, the safety performance of the cold firework medicament is remarkably improved, the safety and the reliability of the cold firework medicament are guaranteed, and an excellent setting-off effect is achieved.

Description

technical field [0001] The invention relates to a heat-stable indoor discharge smokeless and sulfur-free cold fireworks agent and a preparation method thereof, belonging to the field of environment-friendly pyrotechnics. Background technique [0002] The development of cold fireworks is a new trend in the future development of the fireworks industry. It has the advantages of environmental protection and low discharge temperature, and has strong competitiveness in the market; moreover, the advantages of cold fireworks in indoor discharge are incomparable to other fireworks. Whether it is in large-scale fireworks parties, wedding celebrations, stage modeling, or in bars and KTVs, there are always cold fireworks. There is no doubt that cold fireworks have broad market prospects and huge economic benefits. [0003] As we all know, the main ingredients of today's cold smoke flowers are ammonium perchlorate, nitrocellulose and low ignition point metal powder. Its discharge will ...

Claims

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Application Information

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IPC IPC(8): C06B27/00C06B23/00C06B25/32
CPCC06B23/00C06B23/006C06B25/32C06B27/00
Inventor 刘吉平吉伟生于保藏李琪军刘克普周天驰
Owner 江西吉润花炮新材料科技有限公司
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