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31results about "Nitrated pentaerythritol explosive compositions" patented technology

Method and device for preparing nanometer-eutectic energetic material

The invention discloses a method and a device for preparing a nanometer-eutectic energetic material. The method comprises the following steps that an energetic material is dissolved in a good solvent and then is transported into a temperature gradient heating furnace through inert gases in an ultrasonic spray manner, and then nanometer-eutectic energetic material crystals are collected through a high-voltage electrostatic field and the good solvent and the inert gases are cooled and recovered. The device used in the method is formed by sequentially communicating an ultrasonic device, the temperature gradient heating furnace, the high-voltage electrostatic field and a receiving device in a sealing manner. The method can prepare the energetic material crystals with the crystal size being 20-1000nm, is wide in preparation range, and can realize continuous operation. The preparation method is simple in procedures and is easy to operate, reaction conditions are mild and are easily controlled, and the method can be applied to various kinds of eutectic explosives. The crystal grains of the prepared nanometer-eutectic energetic explosives are uniform, and the purity is larger than 99.9 percent. Waste liquid in the preparation procedures is recovered, and the minimum pollution to the environment is realized.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS

Method for preparing ordered porous energetic crystal material

The invention discloses a method for preparing an ordered porous energetic crystal material. The method comprises the following steps of: dissolving a certain amount of energetic materials in a good solvent at room temperature; adding a certain amount of crystal morphology control agents into the solution in the previous step, stirring, dissolving, and slowly adding the solution in the previous step into a poor solvent of the energetic materials and the crystal morphology control agents under the magnetic stirring conditions; continuously stirring the solution in the previous step for a certain time, filtering, and obtaining a composite material of the energetic materials and the crystal morphology control agents; adding the obtained composite material into the solvent, wherein the solvent is a poor solvent of the energetic materials and a good solvent of the crystal morphology control agents; repeatedly washing and removing the crystal morphology control agents; and drying to obtain pure ordered porous energetic crystal material. The preparation method is simple in process flow and mild in reaction conditions and suitable for various energetic materials, the reaction conditions are easy to control, and the prepared ordered porous energetic crystal material has the purity of over 99.5 percent.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS +1

Micro-priming powder for detonator

The invention relates to micro initiating explosive for an exploder, and solves the problems of insecurity of the exploder with the initiating explosive and high cost of the exploder without the initiating explosive. The micro initiating explosive comprises more than one high explosive and more than one initiating explosive. The high explosive comprises hexogen and PETN; the initiating explosive comprises dinitrodiazophenol, lead azide, lead trinitroresorcinate, nickel hydrazine nitrate and perchloric acid tricarbohydrazide cadmium complex; and the more than one high explosive and the more than one initiating explosive are mixed to prepare the micro initiating explosive. Adhesive and surfactant can also be used. The micro initiating explosive has the advantages that the micro initiating explosive can reduce the content of the initiating explosive by 30 to 60 percent compared with the conventional exploder filled with the explosive, lower 20 to 30 percent of cost compared with the prior exploder, improve safety during assembly of the exploder, reduce static electricity, friction, impact and light and heat sensitivity while ensuring initiating force and flame sensitivity, improve safety during production, transportation, storage and use of the exploders, can reduce explosive feeding amount of the exploder, and improve free-running property of preparations.
Owner:ANHUI UNIV OF SCI & TECH

Explosion hardening explosive and preparation method thereof

The invention discloses an explosion hardening explosive and a preparation method thereof. The explosion hardening explosive is prepared from the following raw materials in parts by weight: 40-80 parts of cyclonite and / or pentaerythrite tetranitrate, 10-30 parts of tributyl acetocitrate and 10-30 parts of nitrocotton. The explosion hardening explosive has the beneficial effects that tributyl acetocitrate and nitrocotton as raw materials of the explosion hardening explosive have high intermiscibility; meanwhile, tributyl acetocitrate is non-toxic and is low in volatility; the finished explosive is high in water resistance and plasticity; the explosion hardening explosive contains additives; due to the addition of the additives, the low-temperature plasticity of the explosive is improved, so that the explosive is uniform in density, high in plasticity and easy to tablet; the explosion hardening explosive is stable in explosion property, high in explosion velocity, high in strength, excellent in normal-temperature and low-temperature plasticity, easy to bend and high in in adhesion and application to workpieces under normal temperature and low temperature conditions, and is capable of effectively ensuring the hardening effect of the workpieces.
Owner:HAIDENG TECH SERVICES DALIAN CO LTD

Initiating explosive actuator adopting low detonation velocity charging to reduce incidental impact and pollution

The invention discloses an initiating explosive actuator adopting low detonation velocity charging to reduce incidental impact and pollution. The initiating explosive actuator comprises a short circuit sleeve, an insulating sleeve, a sealant, an electric igniter, a reinforcing ring, a tube shell, a driving explosive, a gasket, a sealing ring and a piston, wherein the electric igniter is composed of an electrode plug, igniting powder, an igniter wire and two conducting wires. The igniting powder is trinitro-resorcinol lead or other weak initiating explosives and ignition powder. The driving explosive is a low-detonation-speed and low-power explosive and can be a hexogen or pentaerythrite tetranitrate-based granular foam explosive, modified black powder, a boron / potassium nitrate ignition explosive, or a pentaerythrite tetranitrate-based PBXN301 mixed explosive and the like. The initiating explosive agent in the traditional initiating explosive actuator is partially or completely replaced by a low-power agent, so that the incidental impact and pollution of the initiating explosive actuator during working can be reduced, the reliability of fuses, ammunition and spacecrafts is improved, and the intrinsic safety of matched products is improved.
Owner:NANJING UNIV OF SCI & TECH

Core of water-resistant detonating cord and method for preparing core

The invention discloses a core of a water-resistant detonating cord and a method for preparing the core. The core comprises, by weight, 15-20 parts of paraffin oil and petroleum ether saturated solution, 79.4-84.6 parts of pentaerythrite tetranitrate and 0.4-0.6 part of graphite powder. The method for preparing the core includes adding the paraffin oil and petroleum ether saturated solution and the graphite powder into the pentaerythrite tetranitrate according to raw material ratios; uniformly stirring and mixing the paraffin oil and petroleum ether saturated solution, the graphite powder andthe pentaerythrite tetranitrate with one another to obtain mixtures; granulating the mixtures; drying granules in water-bath drying tanks at the drying temperatures of 45-50 DEG C to obtain the core of the water-resistant detonating cord. The core and the method have the advantages that formulas for the core are improved, accordingly, the water resistance of the core can be integrally improved, the stability of the core can be reinforced, the storage life can be prolonged, and the explosion initiation and propagation performance of the core can be guaranteed; the water resistance and the stability of the core can be improved to the greatest extent by the aid of the method for preparing the core.
Owner:JIANGXI GANZHOU GUOTAI SPECIALTY CHEM

Method for preparing ordered porous energetic crystal material

The invention discloses a method for preparing an ordered porous energetic crystal material. The method comprises the following steps of: dissolving a certain amount of energetic materials in a good solvent at room temperature; adding a certain amount of crystal morphology control agents into the solution in the previous step, stirring, dissolving, and slowly adding the solution in the previous step into a poor solvent of the energetic materials and the crystal morphology control agents under the magnetic stirring conditions; continuously stirring the solution in the previous step for a certain time, filtering, and obtaining a composite material of the energetic materials and the crystal morphology control agents; adding the obtained composite material into the solvent, wherein the solvent is a poor solvent of the energetic materials and a good solvent of the crystal morphology control agents; repeatedly washing and removing the crystal morphology control agents; and drying to obtain pure ordered porous energetic crystal material. The preparation method is simple in process flow and mild in reaction conditions and suitable for various energetic materials, the reaction conditions are easy to control, and the prepared ordered porous energetic crystal material has the purity of over 99.5 percent.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS +1

Micro-priming powder for detonator

The invention relates to micro initiating explosive for an exploder, and solves the problems of insecurity of the exploder with the initiating explosive and high cost of the exploder without the initiating explosive. The micro initiating explosive comprises more than one high explosive and more than one initiating explosive. The high explosive comprises hexogen and PETN; the initiating explosive comprises dinitrodiazophenol, lead azide, lead trinitroresorcinate, nickel hydrazine nitrate and perchloric acid tricarbohydrazide cadmium complex; and the more than one high explosive and the more than one initiating explosive are mixed to prepare the micro initiating explosive. Adhesive and surfactant can also be used. The micro initiating explosive has the advantages that the micro initiating explosive can reduce the content of the initiating explosive by 30 to 60 percent compared with the conventional exploder filled with the explosive, lower 20 to 30 percent of cost compared with the prior exploder, improve safety during assembly of the exploder, reduce static electricity, friction, impact and light and heat sensitivity while ensuring initiating force and flame sensitivity, improve safety during production, transportation, storage and use of the exploders, can reduce explosive feeding amount of the exploder, and improve free-running property of preparations.
Owner:ANHUI UNIV OF SCI & TECH

Thermostable indoor set-off smokeless sulfur-free cold firework medicament and preparation method thereof

The invention relates to a thermostable indoor set-off smokeless sulfur-free cold firework medicament and a preparation method thereof, and belongs to the field of environment-friendly pyrotechnic compositions. The firework medicament is composed of the components: nano titanium-magnesium powder, modified pentaerythritol tetranitrate, zirconium deuteride, dihydroxy glyoxime, nitrobamboo cellulose,dimethyl diphenyl urea, zinc stearate, nitro tert-butyl triol trinitrate, polyethylene wax and diatomite. The nano magnesium-aluminum powder and the modified pentaerythritol tetranitrate powder are used as main components, so that the setting-off temperature is low, and safety and reliability are realized; dihydroxy glyoxime and zirconium deuteride are introduced, so that sufficient combustion and bright color are ensured; the components do not contain chlorine elements and sulfur elements, so that no toxic and harmful smoke is generated; self-made nitrated bamboo cellulose is adopted, and dimethyl diphenyl urea is introduced, so that the compatibility and the mechanical property of the cold firework medicament can be effectively improved, the safety performance of the cold firework medicament is remarkably improved, the safety and the reliability of the cold firework medicament are guaranteed, and an excellent setting-off effect is achieved.
Owner:江西吉润花炮新材料科技有限公司

Method and device for preparing nanoeutectic energetic material

The invention discloses a method and a device for preparing a nanometer-eutectic energetic material. The method comprises the following steps that an energetic material is dissolved in a good solvent and then is transported into a temperature gradient heating furnace through inert gases in an ultrasonic spray manner, and then nanometer-eutectic energetic material crystals are collected through a high-voltage electrostatic field and the good solvent and the inert gases are cooled and recovered. The device used in the method is formed by sequentially communicating an ultrasonic device, the temperature gradient heating furnace, the high-voltage electrostatic field and a receiving device in a sealing manner. The method can prepare the energetic material crystals with the crystal size being 20-1000nm, is wide in preparation range, and can realize continuous operation. The preparation method is simple in procedures and is easy to operate, reaction conditions are mild and are easily controlled, and the method can be applied to various kinds of eutectic explosives. The crystal grains of the prepared nanometer-eutectic energetic explosives are uniform, and the purity is larger than 99.9 percent. Waste liquid in the preparation procedures is recovered, and the minimum pollution to the environment is realized.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS

Method for flow type ultrasonic processing of intercrystalline acid of single-compound explosive

The invention provides a method for flow type ultrasonic processing of intercrystalline acid of a single-compound explosive, and the method comprises the following steps: mixing an acid-containing single-compound explosive crude product with water to form a mixed material; controlling the temperature in a washer to be kept at 25-45 DEG C; enabling the mixed material to enter from the lower end ofthe washer and flow out from the upper end, circulating for a certain time and then performing ultrasonic processing; in the ultrasonic process, controlling the temperature in the washer not to exceed50 DEG C, circularly washing for a certain time, and stopping ultrasonic processing when the pH value in the washer is stable; and filtering and leaching the washed single-compound explosive product,and drying to obtain the single-compound explosive product meeting the acidity requirement. According to the method, washing water is recycled, energy consumption is low, efficiency is high, mass production is easy to achieve, the energy utilization rate of the ultrasonic effect can be increased through circular flowing of the washing water, meanwhile, water consumption is further reduced, and large-scale application of the method can be achieved through series connection of multiple ultrasonic washers.
Owner:XIAN MODERN CHEM RES INST

A flow-type ultrasonic treatment method for intercrystalline acid in simple explosives

The present invention proposes a flow-type ultrasonic treatment method for the intercrystalline acid of elemental explosives, which comprises taking the crude acid-containing elemental explosives and mixing them with water to form a mixed material; controlling the temperature in the scrubber to keep at 25-45°C; making the mixed material from washing The lower end of the washer enters, the upper end flows out, and ultrasonic treatment is performed after a certain period of circulation; during the ultrasonic process, the temperature in the washer is controlled not to exceed 50°C, and after a certain period of cycle washing, the ultrasonic treatment is stopped when the pH value in the washer is stable; The explosive product is dried after being filtered and rinsed to obtain a simple explosive product meeting the acidity requirement. In this method, the washing water is recycled, the energy consumption is low, the efficiency is high, and it is easy to realize mass production. The method can improve the energy utilization rate of the ultrasonic action through the circulating flow of the washing water, and also further reduce the consumption of water, and the method can be used Large-scale application is realized by connecting multiple ultrasonic scrubbers in series.
Owner:XIAN MODERN CHEM RES INST
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