16 results about "Nonane" patented technology

The application provides a preparation method of 3,7-dinitro-1,3,5,7-tetraazabicyclononane, comprising the following steps: 1) feeding a first material comprising urea and concentrated sulfuric acid and a second material comprising fuming nitric acid and concentrated sulfuric acid into a microchannel reactor to perform a first-stage nitration reaction, to obtain a first-stage nitration reaction liquid; 2) feeding the first-stage nitration reaction liquid into a first tubular reactor to perform a second-stage nitration reaction, to obtain a second-stage nitration reaction liquid; 3) feeding the second-stage nitration reaction liquid and water into a second tubular reactor to perform a hydrolysis reaction, to obtain a hydrolysis liquid; 4) feeding the hydrolysis liquid and a third material comprising polyoxymethylene and ammonia water into a third tubular reactor to perform a condensation cyclization reaction, to obtain 3,7-dinitro-1,3,5,7-tetraazabicyclononane. The preparation method has the advantages of high safety, less waste pollution and simple operation.

This invention discloses an iron complex with a triazacyclic nonane macrocyclic skeleton, its preparation method, and its applications, belonging to the field of coordination chemistry. The iron complex has a triazacyclic nonane macrocyclic skeleton with two acetate side groups and one pyridine-N derivative side group. The iron complex exhibits excellent catalytic activity in the aerobic oxidation of N-aryltetrahydroisoquinoline, while also possessing good stability. The solvents for the catalytic reaction are water and acetonitrile, resulting in low pollution. This invention features mild reaction conditions, simple synthesis operations, and straightforward post-processing, meeting the requirements of environmental friendliness and clean production.

This invention relates to a polyisoprene-based phloroglucinol compound, its preparation method, and its applications, belonging to the field of pharmaceutical technology. The structural formula of the compound is shown below. The preparation method involves extracting the fruit of *Garcinia macrocarpa* in an aqueous organic solvent solution, followed by extraction with petroleum ether and dichloromethane, and then purifying the compound using silica gel column chromatography, ODS column chromatography, Sephadex LH-20 gel column chromatography, and semi-preparative high-performance liquid chromatography. The above method is simple and easy to implement, and the resulting compound has a novel structure with a [2,4,1]nonane core structure. It can promote the secretion of insulin in palmitic acid-induced pancreatic β-cells, showing promise for the preparation of drugs for the prevention and treatment of hyperglycemia.

The invention belongs to the technical field of fine fluorine chemical industry, and discloses a perfluoroalkane dielectric cooling liquid composition with customizable performance and a selective continuous preparation method thereof. The composition is composed of saturated derivatives of hexafluoropropylene oligomer and can comprise a perfluoro-branched hexane isomer mixture, a perfluoro-branched nonane isomer mixture and a perfluoro-branched alkane higher oligomer mixture with the polymerization degree not lower than 7, and key performance such as the boiling range, the viscosity and the freezing point can be customized by regulating and controlling the proportion of all the components. According to the preparation method, an integrated continuous flow system is adopted, and on-demand production of cooling liquid with different component proportions is realized through the steps of controllable initial oligomerization, selectable controllable chain growth and continuous saturation. The product provided by the invention has excellent comprehensive thermophysical properties, is suitable for immersed cooling of high-heat-flux electronic equipment such as an AI data center and a super computer, and has the advantages of high process platformization degree and good economical efficiency.

Provided herein are crystalline forms of 5-(3,4-difluorobenzyl)-8-((1r,4r)-4-methylcyclohexyl)-6,9-dioxo-2,5,8-triazaspiro[3.5]nonane-2-carbaldehyde, compositions thereof, methods of preparation thereof, and methods of their uses.

The invention provides a method for determining the content of a target component in coking crude benzene. The method for determining the content of the target component in the coking crude benzene comprises the following steps: mixing a coking crude benzene sample with internal standard substances 1, 4-dioxane and n-nonane, and injecting the mixture into a chromatographic instrument by adopting a capillary chromatographic column and taking methanol as a mobile phase to obtain a chromatogram and peak areas of all substances; calculating to obtain the content of the target component; the target components comprise benzene, toluene, ethylbenzene and xylene; wherein the xylene comprises p-xylene, m-xylene and o-xylene; the capillary chromatographic column comprises any one of a cross-linked and bonded polyethylene glycol quartz elastic capillary chromatographic column, a DB-1 chromatographic column and an HP-5 chromatographic column. According to the method disclosed by the invention, the component detection in the coking crude benzol is more accurate, the refining processing technology develops towards a more large-scale and multi-product deep processing direction, a higher additional value is generated, and the high-quality development of the industry is promoted.

The present invention provides a novel method for producing 1,9-nonane diol, with which 1,9-nonane diol can be efficiently produced with little environmental burden. This method for producing 1,9-nonane diol includes: (1) a step for blowing ozone gas into oleyl alcohol in such a way that ozone gas is blown until the ozone gas concentration at an outlet exceeds half the ozone gas concentration at an inlet, and the acid value of a treated product that has been treated with the ozone gas is 15 mg KOH / g or less; and (2) a step for hydrogenating, in the presence of a nickel catalyst, the treated product that has been treated with the ozone gas.

The invention discloses a polyurethane elastomer and a preparation method thereof. A soft segment of the polyurethane elastomer comprises polytetrahydrofuran, diisocyanate and 2, 7-diazaspiro [4.4] nonane which are combined to serve as a hard segment, and the 2, 7-diazaspiro [4.4] nonane high-strength polyurethane elastomer is obtained through a prepolymerization and chain extension two-step method. The elastomer is endowed with high glass transition temperature, high mechanical strength, high modulus and high chemical corrosion resistance through the super-rigid three-dimensional space constraint effect of a spiral ring and the strong hydrogen-bond interaction of allophanate.

The invention discloses a preparation method of a moxifloxacin hydrochloride intermediate with high yield, high purity and low cost, and aims to overcome the technical defects of low resolution yield, need of additional acid addition, single solvent system, complex resolution agent recovery process and limited salifying efficiency in the prior art. According to the method, cis-8-benzyl-7, 9-dioxo-2, 8-diazabicyclo [4.3. 0] nonane (a compound as shown in a formula I) is taken as a raw material, N-acetylphenylalanine (including L-type and D-type) is taken as a resolving agent, acid does not need to be additionally added in a water-alcohol-ester ternary solvent system, efficient resolution of the enantiomer is directly realized through a salt forming reaction, and the yield of the enantiomer is increased. And the high-purity diazabicyclo compounds shown in the formulas IIIa and IIIb can be obtained without a refining step. The resolution yield can reach 90% or above, the recovery process of the resolving agent is simple and efficient, the recovery rate is larger than or equal to 95%, the resolving agent can be stably and circularly applied for five times or above, the resolution yield is still larger than or equal to 90% after the resolving agent is applied, the comprehensive production cost is reduced by 40%-60% compared with the prior art, and the method has outstanding industrial application advantages.

The application provides a method for preparing normal paraffin from coal-based hydrorefined naphtha, which comprises the following steps: performing rectification separation on the coal-based hydrorefined naphtha to obtain C6 and above alkane; feeding the C6 and above alkane into a de-normal-hexane rectification tower to obtain crude normal hexane and C7 and above alkane; feeding the C7 and above alkane into a de-normal-heptane rectification tower to obtain crude normal heptane and C8 and above alkane; feeding the C8 and above alkane into a de-normal-octane rectification tower to obtain crude normal octane and C9 and above alkane; feeding the C9 and above alkane into a de-normal-nonane rectification tower to obtain crude normal nonane and C10 and above alkane; and performing rectification and deep hydrogenation on each crude normal paraffin to obtain normal hexane product, normal heptane product, normal octane product and normal nonane product. The technical scheme of the application uses coal-based hydrorefined naphtha as raw material, has a simple process flow and low energy consumption, and overcomes the problem of single product structure in the prior art.

The application provides a high-pressure liquid supply system, comprising a low-pressure pipeline module, a high-pressure pump module, a high-pressure pipeline module and a control module; the low-pressure pipeline module comprises a liquid inlet pipeline and a liquid return pipeline, the inlet of the liquid inlet pipeline and the outlet of the liquid return pipeline are connected to a liquid source, and the outlet of the liquid inlet pipeline is connected to the inlet of the high-pressure pump module; the outlet of the high-pressure pump module is connected to the high-pressure pipeline module, so that the high-pressure pump module is used for pressurizing the inflowing liquid; the high-pressure pipeline module comprises multiple loops, one of which is used for supplying liquid to a demand side, and the other loops are connected to the liquid return pipeline after being combined; and the control module is used for controlling the working states of the low-pressure pipeline module, the high-pressure pump module and the high-pressure pipeline module. The application can realize automatic supply of high-pressure n-nonane liquid, realize real-time monitoring of temperature, pressure control and flow data of n-nonane, and achieve unattended operation.

The application discloses a water-based electrolyte and a zinc ion hybrid capacitor comprising the water-based electrolyte. The water-based electrolyte is a water-based electrolyte for a zinc ion hybrid capacitor, and comprises a zinc salt, an electrolyte additive and water. The electrolyte additive comprises a first additive and a second additive. The first additive is an organic antifreezing agent, and the second additive is a heterocyclic nonane. The volume fraction of the organic antifreezing agent in the water-based electrolyte is greater than 0.1% and less than 40%. The water-based electrolyte of the application uses the organic antifreezing agent and the heterocyclic nonane as additives, and the two cooperate with each other. The water-based electrolyte can not only prevent freezing and avoid ice formation, but also modify the zinc negative electrode interface, reduce the Zn 2+ reduction rate, alleviate concentration polarization, thereby facilitating inhibition of dendrite growth, and can also inhibit the side reaction of the zinc negative electrode, thereby improving the low-temperature cycle performance of the zinc ion hybrid capacitor.