A kind of bifunctional chemical warfare agent degradation material and its preparation method
A chemical warfare agent and degradable material technology, which is applied in the field of dual-functional chemical warfare agent degradation materials and its preparation, can solve problems such as unpredictable chemical warfare agent types, and achieve the effect of great application value
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Embodiment 1
[0031](1) Dissolve 12g of aluminum chloride hexahydrate in 200mL of deionized water to obtain a 0.25mol / L aluminum chloride hexahydrate solution after dissolving;
[0032] (2) stirring the solution obtained in step (1) at 80°C;
[0033] (3) 4.5g sodium hydroxide is dissolved in the deionized water of 450mL, obtains the sodium hydroxide solution of 0.25mol / L;
[0034] (4) Slowly add the sodium hydroxide solution obtained in step (3) dropwise to the aluminum chloride hexahydrate solution obtained in step (1) to obtain Al 13 7+ solution;
[0035] (5) the Al obtained in step (4) 13 7+ The solution uses deionized water as a solvent, and is configured to obtain Al with a concentration of 6mmol / L 13 7+ solution, take 20mL of Al after configuration 13 7+ solution;
[0036] (6) H 5 PV 2 Mo 10 o 40 Dissolve in deionized water and configure to obtain H with a concentration of 6mmol / L 5 PV 2 Mo 10 o 40 solution, take 20mL of prepared H 5 PV 2 Mo 10 o 40 solution;
[...
Embodiment 2
[0040] (1) Dissolve 12g of aluminum chloride hexahydrate in a mixed solution of 200mL ethanol and tetrahydrofuran to obtain a 0.25mol / L aluminum chloride hexahydrate solution after dissolving;
[0041] (2) stirring the solution obtained in step (1) at 80°C;
[0042] (3) 4.5g sodium hydroxide is dissolved in the deionized water of 450mL, obtains the sodium hydroxide solution of 0.25mol / L;
[0043] (4) Slowly add the sodium hydroxide solution obtained in step (3) dropwise to the aluminum chloride hexahydrate solution obtained in step (1) to obtain Al 13 7+ solution;
[0044] (5) the Al obtained in step (4) 13 7+ The solution uses a mixed solution of ethanol and tetrahydrofuran as a solvent, and is configured to obtain Al with a concentration of 6mmol / L. 13 7+ solution, take 20mL of Al after configuration 13 7+ solution;
[0045] (6) H 3 PMo 12 o 40 Dissolve in a mixed solution of ethanol and tetrahydrofuran, and configure to obtain H with a concentration of 6mmol / L ...
Embodiment 3
[0049] (1) Dissolve 12g of aluminum chloride hexahydrate in 200mL of N,N-dimethylformamide, and obtain a 0.25mol / L aluminum chloride hexahydrate solution after dissolving;
[0050] (2) stirring the solution obtained in step (1) at 80°C;
[0051] (3) 4.5g sodium hydroxide is dissolved in the deionized water of 450mL, obtains the sodium hydroxide solution of 0.25mol / L;
[0052] (4) Slowly add the sodium hydroxide solution obtained in step (3) dropwise to the aluminum chloride hexahydrate solution obtained in step (1) to obtain Al 13 7+ solution;
[0053] (5) the Al obtained in step (4) 13 7+ The solution uses N,N-dimethylformamide as solvent, and configures Al with a concentration of 6mmol / L 13 7+ solution, take 20mL of Al after configuration 13 7+ solution;
[0054] (6) H 3 PW 12 o 40 Dissolved with N,N-dimethylformamide, and configured to obtain H with a concentration of 6mmol / L 3 PW 12 o 40 solution, take 20mL of prepared H 3 PW 12 o 40 solution;
[0055] (...
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