Rare earth based magnetic skyrmions material as well as preparation method and application thereof
A magnetic skyrmion, rare earth-based technology, applied in static memory, instruments, digital memory information and other directions, can solve the problems of low phase transition temperature, high cost, high technical difficulty, etc., and achieves simple preparation method, low cost, and composition. controllable effect
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Embodiment 1
[0018] This embodiment prepares the magnetic skyrmion material of chemical formula Nd20Mn40Ge40, and its preparation method is carried out according to the following specific steps:
[0019] Step 1: According to the molar ratio Nd:Mn:Ge=20:40:40 ratio, respectively weigh Nd, Mn, Ge raw materials with a purity of 99.9%;
[0020] Step 2: Put the weighed raw materials into a water-cooled crucible, and under the protection of Ar gas, heat the raw materials melted by electric arc until melting and keep for 1 minute;
[0021] Step 3: Turn over the product obtained in Step 2, heat it again by arc melting until it melts, and keep it for 1 minute, repeat this step 3 times;
[0022] Step 4: heating the obtained Nd20Mn40Ge40 ingot to 600 degrees Celsius and annealing under vacuum for 48 hours to obtain a polycrystalline block.
[0023] Using magnetic measurements and Lorentz electron microscopy to test the above-obtained bulk, it is shown that the material forms stable skyrmion magnetic...
Embodiment 2
[0025] This embodiment prepares the magnetic skyrmion material of chemical formula Pr22Mn38Ge40, and its preparation method is carried out according to the following specific steps:
[0026] Step 1: According to the ratio of Pr:Mn:Ge=22:38:40 in molar ratio, respectively weigh Pr, Mn, Ge raw materials with a purity of 99.9%;
[0027] Step 2: Put the weighed raw materials into a water-cooled crucible, and under the protection of Ar gas, heat the raw materials for induction melting until melting and keep for 2 minutes;
[0028] Step 3: Turn over the product obtained in Step 2, heat it again by arc melting until it melts, and keep it for 1 minute;
[0029] Step 4: heating the obtained Pr22Mn38Ge40 ingot to 900 degrees Celsius and annealing under vacuum for 68 hours to obtain a polycrystalline block.
[0030] Using magnetic measurement and Lorentz electron microscopy to test the above-obtained bulk body, it is shown that the material has a skyrmion magnetic domain structure in th...
Embodiment 3
[0032] This embodiment prepares the magnetic skyrmion material of chemical formula Yb12La10Mn35Ge39Fe2Si2, and its preparation method is carried out according to the following specific steps:
[0033] Step 1: According to the ratio of molar ratio Yb:La:Mn:Ge:Fe:Si=12:10:35:39:2:2, respectively weigh Yb, La, Mn, Ge, Fe, Si raw material;
[0034] Step 2: Put the weighed raw materials into a water-cooled crucible, and under the protection of Ar gas, heat the raw materials melted by electric arc until melting and keep for 1 minute;
[0035] Step 3: Turn over the product obtained in Step 2, heat it again by arc melting until it melts, and keep it for 3 minutes, repeat this step 3 times;
[0036] Step 4: heating the obtained Yb12La10Mn35Ge39Fe2Si2 ingot to 200 degrees Celsius and annealing under vacuum for 48 hours to obtain a polycrystalline block.
[0037] Using the magnetic measurement and the Lorentz electron microscope to test the above obtained block, it shows that the Yb20M...
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