Preparation process of high-uniformity conductive silicon target material

A preparation process and uniformity technology, which is applied in the field of high uniformity conductive silicon target preparation technology, can solve the problems of uneven powder composition, uneven doping amount, complicated process, etc., and achieve uniform resistivity and uniform doping content. , the effect of short production cycle

Inactive Publication Date: 2020-04-28
SOLERAS ADVANCED COATINGS (JIANGYIN) CO LTD
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  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, the thermal spraying process produces target materials. The pretreatment of raw materials is divided into mechanical mixing process and melting casting doping process. If mechanical mixing is used, there will be problems such as uneven doping amount and large loss during the spraying process of dopant. The melting and casting doping process is complex and costly, and the powder also has the problem of uneven composition

Method used

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Embodiment Construction

[0014] The invention relates to a high-uniformity conductive silicon target preparation process, the process steps are:

[0015] Step 1: Prepare materials: put high-purity silicon powder and boron powder according to the proportion of boron concentration of 20-200ppm; among them, the purity of silicon powder is 99.99%, the particle size is 20-180um, the purity of boron powder is 99.9%, and the particle size is 20 ~100um;

[0016] Step 2: Grinding: Use a mechanical ball mill to mill the mixture of step 1; before grinding, vacuum the ball mill chamber of the mechanical ball mill and fill it with argon gas. The mixture in No. 1 is started to be ball-milled, the ball-milling speed is 600-1200RPM, and the ball-milling time is 6-8 hours; among them, the grinding balls are made of zirconia with high hardness;

[0017] Step 3: Spray granulation: import the powder with a particle size of 1-10um after step 2 into a spray granulation dryer for granulation to obtain spherical milled powd...

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Abstract

The invention relates to a preparation process of a high-uniformity conductive silicon target material. The preparation process comprises the following steps of 1, preparing materials, specifically, high-purity silicon powder and boron powder are added according to the proportion that the boron concentration content is 20-200 ppm; 2, grinding, specifically, ball milling is carried out on the mixture obtained in step 1 by using a mechanical ball mill; 3, spray granulating, specifically, the powder, with the particle size of 1-10 micros, ground in the step 2 is introduced into a spray granulation dryer for granulating, and spherical ground powder with the particle size of 40-160 micros is obtained; and 4, vacuum spraying, specifically, the spherical powder obtained in the step 3 is sprayed on the surface of a target material base material in a low vacuum environment by means of a plasma spraying mode. According to the preparation process of the high-uniformity conductive silicon target material, the quality of the target material is effectively improved, and the cost is reduced.

Description

technical field [0001] The invention relates to a high-uniformity conductive silicon target preparation process. Background technique [0002] At present, the thermal spraying process produces target materials. The pretreatment of raw materials is divided into mechanical mixing process and melting casting doping process. If mechanical mixing is used, there will be problems such as uneven doping amount and large loss during the spraying process of dopant. The melting and casting doping process is complex and costly, and the powder also has the problem of uneven composition. Contents of the invention [0003] The purpose of the present invention is to overcome the above disadvantages and provide a high-uniformity conductive silicon target preparation process, which effectively improves the quality of the target and reduces the cost. [0004] The purpose of the present invention is achieved like this: [0005] A high-uniformity conductive silicon target preparation process,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C4/04C23C4/134C23C4/137
CPCC23C4/04C23C4/134C23C4/137
Inventor 蔺裕平韩刚库
Owner SOLERAS ADVANCED COATINGS (JIANGYIN) CO LTD
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