Preparation process of high-uniformity conductive silicon target material
A preparation process and uniformity technology, which is applied in the field of high uniformity conductive silicon target preparation technology, can solve the problems of uneven powder composition, uneven doping amount, complicated process, etc., and achieve uniform resistivity and uniform doping content. , the effect of short production cycle
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[0014] The invention relates to a high-uniformity conductive silicon target preparation process, the process steps are:
[0015] Step 1: Prepare materials: put high-purity silicon powder and boron powder according to the proportion of boron concentration of 20-200ppm; among them, the purity of silicon powder is 99.99%, the particle size is 20-180um, the purity of boron powder is 99.9%, and the particle size is 20 ~100um;
[0016] Step 2: Grinding: Use a mechanical ball mill to mill the mixture of step 1; before grinding, vacuum the ball mill chamber of the mechanical ball mill and fill it with argon gas. The mixture in No. 1 is started to be ball-milled, the ball-milling speed is 600-1200RPM, and the ball-milling time is 6-8 hours; among them, the grinding balls are made of zirconia with high hardness;
[0017] Step 3: Spray granulation: import the powder with a particle size of 1-10um after step 2 into a spray granulation dryer for granulation to obtain spherical milled powd...
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