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240 results about "Boron concentration" patented technology

Concentrations of boron in surface water range widely, from 0.001 mg/litre to as much as 360 mg/litre. However, average boron concentrations are typically well below 0.6 mg/litre (see table below).

Method for preparing high-purity magnesium oxide with high boron salt lake brine

Provided is a method for preparing high-purity magnesium oxide with high boron salt lake brine. Salt lake brine is evaporated through a salt pan, concentrated to crystallize potassium sulfate, sodium chloride and potassium chloride and is drawn with lithium in adsorption mode so as to obtain master sauce brine containing magnesium and boron. Concentrated sulfuric acid is added into master sauce brine for reacting, and coarse boracic acid and acidized brine are obtained after cooling and filtering. Potential of hydrogen (pH) value of acidized brine is adjusted to be 5.5-6.5, and acidized brine passes through ion exchange resin adsorbing boron. When boron concentration in effluent liquid is higher than 5 mg / L, brine is not injected, boron-removed brine is obtained, then boron-removed brine and ammonium chloride solution are filled with ammonia for stirring and to produce magnesium sedimentation reaction, reaction temperature ranges from 60 DEG C to 80 DEG C, pH ranges from 7.5 to 8.0, the reaction is stopped when concentration of free ammonia reaches 1.8-2.2 mol / L, and magnesium hydroxide and magnesium sedimentation mother solution are obtained. Magnesium oxide is obtained by calcining magnesium hydroxide, content of magnesium oxide is larger than 99.8%, and magnesium extraction ratio is larger than 90%. Sedimentation mother solution adopts lime to steam ammonia, and generated ammonia circulates to magnesium sedimentation reaction. Mother solution after ammonia steaming is evaporated, concentrated and crystallized to obtain calcium chloride. Ion exchange resin adsorbing boron is washed, analyzed and regeneratively cycled for use. Boron-containing analysis solution is concentrated and cooled to pick up coarse boracic acid, and coarse boracic acid is recrystallized to obtain refined boracic acid with purity larger than 99%. High-purity magnesium oxide prepared by the method is high in purity, good in economic benefit, free of environment pollution, strong in operability and favorable for industrial production.
Owner:CENT SOUTH UNIV

Method for determining boron content in rubber

The invention discloses a method for determining boron content in rubber. The method employs a graphite furnace atomic absorption spectrometry method for determination and calculation of boron content in rubber. The method comprises steps of: conducting pretreatment on a rubber sample; conducting high-temperature ashing by a muffle furnace; adding a mixed acid of hydrofluoric acid and concentrated sulfuric acid in the ash; digesting, drying and placing the ash in the muffle furnace; calcining at 800 DEG C; dissolving the ash with hydrochloric acid to gain a transparent sample solution, and conducting a blank test with the sample; preparing a boron standard work solution above 4 point by using a boron standard stock solution; adding a matrix modifier Ca (NO3) 2 with a same concentration into the sample solution, the blank solution and the standard work solution, and adding high purity water for constant volume; optimizing test conditions of the graphite furnace atomic absorption spectrometry, measuring boron absorbance of the sample solution, the blank solution and the standard solution, and drawing a standard working curve to obtain boron concentration in the sample solution; and calculating the content (in percentage) of boron in the rubber sample. The determination method has advantages of results with high precision and accuracy.
Owner:BEIJING RES & DESIGN INST OF RUBBER IND

Method for preventing abnormity of mechanical seal leakage rate of nuclear reactor coolant pump

The invention relates to a method for preventing abnormity of mechanical seal leakage rate of a nuclear reactor coolant pump. An injection water loop of a No. 1 shaft seal of a coolant pump is provided with two parallel columns of filters; one row of the filters are operating on the line, and the other column of filters are for standby. The preventive method comprises the following steps: S1. detecting a boron concentration of a loop; S2. comparing the boron concentration of the loop with that of the row of filters for standby; and S3. when a difference between the boron concentration of the standby row and that of the loop exceeds a preset value, switching the standby column of filters to on-line operation, and switching the on-line operating row of filters into a standby state. In the preventive method of the invention, when the difference between the boron concentration of the standby column and that of the loop exceeds the preset value, filter switching is carried out; and a sealing surface of the No. 1 shaft seal can be flushed timely by shaft seal injection water with a relative high boron concentration in the standby column of filters, so as to improve a seal status of the sealing surface of the No. 1 shaft seal timely and effectively.
Owner:GUANGDONG NUCLEAR POWER JOINT VENTURE +1

Boron concentration meter for nuclear power station and calibration method thereof

InactiveCN103680650ARealize online real-time monitoringSolve the problem of boron concentration measurement driftNuclear energy generationNuclear monitoringObservational errorMeasurement device
The invention discloses a boron concentration meter for a nuclear power station and a calibration method thereof. A detection device of the boron concentration meter is characterized in that a section of pipe on a drainage water monitoring branch is taken as a sampling pipe which serves as a sharing pipe section of a to-be-measured water monitoring branch and a calibration loop, and on-line communication of the sampling pipe and the calibration loop is realized through switching of tee branch control valves at two ends of the sharing pipe section; chemical titration as a standard, and the calibration for the boron concentration meter is finished ; and the operation is transferred to the monitoring branch after the calibration for real-time monitoring of boron concentration of primary loopwater . A measuring device adopts a linear mathematic model to establish a measurement relation in a piecewise fitting manner, so that the measurement precision is improved; and by means of an established on-line immediate calibration method, measurement drifting is eliminated, and measurement errors are corrected. The device is simple in structure, the measurement method is accurate and reliable, and the operation is easy; and by virtue of the calibration method, the insurmountable technical problem caused by enlargement of measurement errors of the boron concentration meter as time goes by is successfully solved, and accurate continuous on-line monitoring of the boron concentration of the primary loopwater is realized.
Owner:阴国玮
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