Preparation method of a self-assembled porous polyaniline/cobalt core-shell spherical structure absorbing material
A spherical structure and wave-absorbing material technology, applied in the field of materials, can solve the problems of poor bonding between cobalt and polyaniline, single loss mechanism, and limited wave-absorbing effect, so as to promote uniform dispersion, enhance electromagnetic wave absorption, and enhance multiple reflections and scattering Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0037] This example provides a method for preparing a self-assembled porous polyaniline / cobalt core-shell spherical structure absorbing material:
[0038] Step 1, dissolving aniline in an organic solvent to form an oil phase suspension.
[0039] Specifically, aniline is purified by distillation under reduced pressure, such as figure 1 As shown, then, the purified aniline was dissolved in carbon tetrachloride organic solvent, the concentration of aniline was 0.05mol / L, stirred for 1h, and the stirring speed was 50rpm, to obtain an oil phase suspension with uniform dispersion of aniline.
[0040] Step 2, performing surface modification with a silane coupling agent and nitration surface modification on the cobalt powder to obtain a modified cobalt powder whose surface is rich in amino groups.
[0041] The specific method of modification is:
[0042] Step a. Prepare 50mL mixed solution according to the volume fraction of ethanol: water = 9:1, add 2g of cobalt powder into the sol...
Embodiment 2
[0053] This example provides a method for preparing a self-assembled porous polyaniline / cobalt core-shell spherical structure absorbing material:
[0054] Step 1, dissolving aniline in an organic solvent to form an oil phase suspension.
[0055] Specifically, aniline is purified by distillation under reduced pressure, such as figure 1 As shown, then, the purified aniline was dissolved in carbon tetrachloride organic solvent, the concentration of aniline was 0.5mol / L, stirred for 1h, and the stirring speed was 50rpm, to obtain an oil phase suspension with uniform dispersion of aniline.
[0056] Step 2, performing surface modification with a silane coupling agent and nitration surface modification on the cobalt powder to obtain a modified cobalt powder whose surface is rich in amino groups.
[0057] The specific method of modification is:
[0058] Step a. Prepare 50mL mixed solution according to the volume fraction of ethanol: water = 9:1, add 2g of cobalt powder into the solu...
Embodiment 3
[0069] This example provides a method for preparing a self-assembled porous polyaniline / cobalt core-shell spherical structure absorbing material:
[0070] Step 1, dissolving aniline in an organic solvent to form an oil phase suspension.
[0071] Specifically, aniline is purified by distillation under reduced pressure, such as figure 1 As shown, then, the purified aniline was dissolved in carbon tetrachloride organic solvent, the concentration of aniline was 1mol / L, stirred for 1h, and the stirring speed was 50rpm, to obtain an oil phase suspension with uniform dispersion of aniline.
[0072] Step 2, performing surface modification with a silane coupling agent and nitration surface modification on the cobalt powder to obtain a modified cobalt powder whose surface is rich in amino groups.
[0073] The specific method of modification is:
[0074] Step a. Prepare 50mL mixed solution according to the volume fraction of ethanol: water = 9:1, add 2g of cobalt powder into the soluti...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com