A nickel-containing composite wave-absorbing material and its preparation method
A composite wave-absorbing material and material liquid technology, which is applied in the field of nickel-containing composite wave-absorbing materials and its preparation, can solve the problems of limiting the application of graphene wave-absorbing materials and narrow graphene absorption frequency bandwidth
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[0038] The present invention also provides a preparation method of the composite wave-absorbing material described in the above technical solution, comprising the following steps:
[0039] (1) Ferric chloride, nano-nickel powder, surfactant, urea and ethylene glycol are mixed to obtain a mixed material liquid;
[0040] (2) mixing the mixed feed liquid obtained in the step (1) with graphene oxide, and carrying out hydrothermal reaction to obtain a hydrothermal reaction feed liquid;
[0041] (3) removing the supernatant of the hydrothermal reaction feed liquid obtained in the step (2), and performing centrifugal washing and drying on the remaining feed liquid in sequence to obtain a composite wave-absorbing material.
[0042] The invention mixes ferric chloride, nano-nickel powder, surfactant, urea and ethylene glycol to obtain a mixed material liquid. In the present invention, the particle size of the nano-nickel powder is consistent with the particle size of the nano-nickel i...
Embodiment 1
[0062] According to the mass ratio of 1:3:2:110:18, weigh graphite powder, potassium permanganate, sodium nitrate, concentrated sulfuric acid and orthophosphoric acid, wherein the mass of concentrated sulfuric acid is crushed to 98%, and the mass concentration of orthophosphoric acid is 1.685g / mL; then after ultrasonically mixing graphite powder, potassium permanganate, sodium nitrate, concentrated sulfuric acid and orthophosphoric acid, the mixture was added to a polytetrafluoroethylene-lined autoclave, and kept at 50°C for 12 hours . After the obtained product was cooled, hydrogen peroxide (the mass fraction of hydrogen peroxide was 30%) was slowly added to it at a rate of 10 mL / min according to the mass ratio of the original graphite powder and hydrogen peroxide at 1:2, and the liquid turned bright yellow. The reacted mixed liquid is washed by distilled water for several times by centrifugation, and the supernatant is discarded after each washing, and then the remaining li...
Embodiment 2
[0069] According to the mass ratio of 1:2:1:90:10, weigh graphite powder, potassium permanganate, sodium nitrate, concentrated sulfuric acid and orthophosphoric acid, wherein the mass of concentrated sulfuric acid is crushed to 98%, and the mass concentration of orthophosphoric acid is 1.685g / mL; then after ultrasonically mixing graphite powder, potassium permanganate, sodium nitrate, concentrated sulfuric acid and orthophosphoric acid, the mixture was added to a polytetrafluoroethylene-lined autoclave, and kept at 60°C for 12 hours . After the obtained product was cooled, hydrogen peroxide (the mass fraction of hydrogen peroxide was 30%) was slowly added to it at a rate of 10 mL / min according to the mass ratio of the original graphite powder and hydrogen peroxide at 1:2, and the liquid turned bright yellow. The reacted mixed liquid is washed by distilled water for several times by centrifugation, and the supernatant is discarded after each washing, and then the remaining liq...
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