High-permeability ferrite magnetic material and preparation method thereof
A technology of magnetic materials and high magnetic permeability, applied in the direction of magnetic materials, inductance/transformer/magnet manufacturing, magnetic objects, etc., to achieve the effects of high practicability, wide application, and reasonable process design
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Embodiment 1
[0037] Comparative example 1:
[0038] Take isocyanate-modified graphene oxide, ordinary carbon nanotubes and deionized water, ultrasonically disperse for 1-1.5h, then add compound A, ultrasonically oscillate for 20-25min, transfer to an autoclave, and treat at 180-200°C for 18- After 20 hours, take it out, wash it, and centrifugally dry it to obtain the finished product.
[0039] In this embodiment, the raw materials of each component of the magnetic material include, by weight, 15-25 parts of modified ferrite, 3-5 parts of modified carrier, 6-8 parts of isocyanate-modified graphene oxide, ordinary carbon 4-7 parts of nanotubes;
[0040] Comparative Example 1 is improved on the basis of Example 2. Common carbon nanotubes are added in Comparative Example 1, and the remaining process parameters and component contents are consistent with Example 2.
[0041] The sample prepared in Comparative Example 1 has a frequency bandwidth of 7.1-14.7 GHz in which the reflectance loss valu...
Embodiment 2
[0050] The sample prepared in Comparative Example 3 has a frequency bandwidth in which the reflectance loss value is lower than -10dB in 2-18GHz is 8.9-12.4GHz, and the minimum reflectance loss value can reach -45.2dB.
[0051] Comparative example 4:
[0052] Take acidified carbon nanotubes and anhydrous toluene, ultrasonically disperse them in a nitrogen environment for 0.5-1h, add toluene diisocyanate and tin catalyst in an oil bath at 60-65°C, stir and react for 8-10h, filter and wash with suction, and dry in vacuum to obtain isocyanate-modified permanent carbon nanotubes.
[0053] Take isocyanate-modified graphene oxide, isocyanate-modified carbon nanotubes and deionized water, ultrasonically disperse for 1-1.5h, then add compound A, ultrasonically oscillate for 20-25min, transfer to an autoclave, and treat at 180-200°C 18-20h, take out and wash, centrifuge and dry to get the finished product.
[0054] In this embodiment, the raw materials of each component of the magnet...
Embodiment 3
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