Optimization method of ardealite-based cementing material for improving filling roof-contacted rate

An optimization method, a technology of phosphogypsum, applied in the direction of material analysis, design optimization/simulation, application, etc., can solve the problems of difficulty in meeting the mining early strength requirements, poor gelation, and low activity of the downward layered filling method, and achieve the realization of Utilization of high-value resources, control of expansion rate, and low material cost

Active Publication Date: 2020-05-22
HEBEI IRON & STEEL GRP MINING +1
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  • Abstract
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  • Claims
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Problems solved by technology

[0003] Harmful mineral components in phosphogypsum lead to low activity, poor gelation, and volume instability, resulting in less than 5% utilization of phosphogypsum
This treatment can improve its early strength to a certain extent, but there is no reliable basis for the significance of the effect, and it is difficult to meet the early strength requirements of the downward layered filling method.
CN108191365A discloses a method of applying phosphogypsum material to cement and fill metal mines. Phosphogypsum is used as a filling cementitious material, and a fill

Method used

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  • Optimization method of ardealite-based cementing material for improving filling roof-contacted rate
  • Optimization method of ardealite-based cementing material for improving filling roof-contacted rate
  • Optimization method of ardealite-based cementing material for improving filling roof-contacted rate

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Embodiment

[0044] Embodiment: The optimization method of this phosphogypsum-based cementitious material is specifically described as follows.

[0045] 1. The activator ratio optimization of early-strength phosphogypsum-based cementitious materials adopts the following steps:

[0046] (1) Dry and grind low-quality phosphogypsum solid waste, and conduct physical and chemical analysis and particle size testing. The results of mineral composition analysis of phosphogypsum are shown in Table 1, and the particle size gradation distribution curve is shown in Table 1. figure 1 , the microscopic surface morphology of phosphogypsum see figure 2 , see the XRD pattern of phosphogypsum image 3 .

[0047] Table 1: Analysis results of mineral composition of phosphogypsum solid waste

[0048]

[0049] (2) Grind and test the particle size of the quicklime activator to obtain the characteristic value of the particle size distribution of quicklime: d 10 =2.17μm, d 30 =4.60μm, d 60 =6.53μm, d 5...

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Abstract

The invention discloses an optimization method of an ardealite-based cementing material for improving the filling roof-contacted rate, comprising the following steps: adding ardealite powder and an excitant in different proportions into filling aggregate to prepare cemented filling body materials in different proportions; carrying out a cemented filling body strength test and a filling body expansion rate test on the cemented filling body materials with different proportions to obtain test data of the cemented filling body strength and the expansion rate of the cemented filling body materialswith different proportions; conducting stepwise regression analysis on the test data of the strength and the expansion rate of the cemented filling body through a quadratic polynomial; establishing aproportion optimization model of the cementing material by taking the 3d strength of the cemented filling body as an optimization target and the 28d filling body expansion rate as a constraint condition; and solving the optimization model to obtain the optimal proportion of the ardealite-based cementing material in the filling slurry. According to the design method, low-cost and high-value resource utilization of ardealite can be realized; and low-cost and high-value utilization of ardealite in filling mining can be realized.

Description

technical field [0001] The invention belongs to the technical field of filling and mining, in particular to an optimization method for a phosphogypsum-based cementitious material that improves the rate of filling and roof connection. Background technique [0002] With the rapid development of my country's national economy and the continuous development of resources, high-grade and good-condition resources are increasingly depleted, and more difficult-to-mine ore bodies such as deep burial, high ground pressure, and rich water are faced with mining. For safety, environmental protection and green mining, the filling and filling mining method is the first choice. Especially for complex and difficult-to-mining ore bodies with weak and broken surrounding rocks, it is necessary to protect them under the false roof of the filling body to achieve safe operation, so the downward layered filling mining method is the only choice. This filling mining method has complicated mining proce...

Claims

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Application Information

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IPC IPC(8): G06F30/20C04B28/14G01N33/00G01N3/00
CPCC04B28/143C04B2111/00724C04B2201/50G01N3/00G01N33/00C04B18/12A47J41/0011C04B22/064C04B22/062C04B22/085
Inventor 黄笃学郭斌杨晓炳温震江闫满志路燕泽李胜辉尹升华陈彦亭胡亚军高谦涂光富高玉倩谢广峰
Owner HEBEI IRON & STEEL GRP MINING
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