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Porous preform, preparation method thereof, foam metal and preparation method thereof

A metal foam and prefabricated technology, applied in the field of metal foam, can solve the problems of poor opening degree, limited contact area, large flow resistance, etc., achieve the effect of simple production method and equipment, increase the size of the connecting hole, and improve the connecting structure

Active Publication Date: 2020-06-05
TSINGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this process also has some inherent disadvantages: First, the porosity of metal foam is approximately equal to the packing rate of the porous preform, but limited by the packing rate of particles, usually the porosity of metal foam prepared by this method does not exceed 70%. %; In addition, the connection channels between the metal foam cells originate from the contact surface between the preform particles, but due to the limited contact area between the particles, the opening degree of the final metal foam is poor, and the flow resistance is relatively low. On the one hand, it limits its functional application, on the other hand, it makes it difficult to remove salt particles, and the unremoved salt particles will cause serious corrosion to the substrate. These factors greatly limit its lightweight and functional applications.
(B) Particle surface treatment, spraying the binder on the surface of the particles, so that the particles overlap with each other, thereby increasing the accumulation rate of the preform, but the bonding between the particles is difficult to control, and it is easy to cause the preform to partially dissolve together. Cause localized defects in the final metal foam
(C) Artificial granulation, making soft granules mechanically or manually according to a certain formula, so as to improve the compressibility of granules, but this method is time-consuming and the granulation efficiency is too low
[0006] In summary, the problems of low porosity and poor opening degree of the open-cell metal foam prepared by the particle infiltration method have not been effectively solved, which limits the large-scale industrial application of this method.

Method used

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  • Porous preform, preparation method thereof, foam metal and preparation method thereof
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  • Porous preform, preparation method thereof, foam metal and preparation method thereof

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preparation example Construction

[0034] An embodiment of the present invention provides a method for preparing a porous preform, comprising the following steps:

[0035]S100, stacking the inorganic salt particles in a container with a closed bottom to form an accumulation of inorganic salt particles;

[0036] S200, using a compaction method to make the inorganic salt particle accumulation body have a preliminary compactness in the container;

[0037] S300, apply a downward constant pressure of 1 MPa to 10 MPa above the accumulation of inorganic salt particles, and raise the temperature of the container containing the accumulation of inorganic salt particles to 0.2Tm to 0.2Tm at a heating rate of 5°C to 20°C. 0.8Tm and heat preservation;

[0038] S400, keeping the temperature for 1 hour to 8 hours, causing the inorganic salt particles to creep and deform.

[0039] The preparation method of the porous prefabricated body in the embodiment of the present invention controls the pressure, temperature, and time. B...

Embodiment 1

[0067] Step 1, preparation of porous preform.

[0068] In this example, industrial pure aluminum is selected as the metal raw material, and CaCl 2 As inorganic salt particles. After particle sieving, CaCl 2 The particle diameter of the particles was 3.5 mm. see figure 1 , assemble the lower pressure head to the bottom of the hollow cylindrical cylinder as a container for standby, and put the sieved CaCl 2 The particles are piled into the container to form an accumulation of inorganic salt particles, and manual vibration and pressure compaction are used to make the inorganic salt particles have a preliminary degree of compaction. The quality of the upper pressure head is 5Kg, which is pressed on the upper surface of the inorganic salt particle accumulation body, and the CaCl 2 The particle container was placed in a heating furnace, and the heating furnace was heated to 550° C. at a heating rate of 10° C. and kept for 2 hours. Take out the container, and take out the porou...

Embodiment 2

[0075] Step 1, preparation of porous preform.

[0076] In this example, industrial pure tin is selected as the metal raw material, and KCl is selected as the inorganic salt particles. After particle sieving, the particle size of the KCl particles was 2.5 mm. Assemble the lower pressure head to the bottom of the hollow cylindrical cylinder as a container for standby, accumulate the sieved KCl particles into the container to form an accumulation of inorganic salt particles, and use manual vibration and pressure compaction to make the inorganic salt particles have a preliminary tightness. Solidity. The mass of the upper pressure head is 10Kg, which is pressed on the upper surface of the inorganic salt particle accumulation body, the container containing the KCl particles is placed in the heating furnace, and the heating furnace is heated to 500°C at a heating rate of 15°C and kept for 1h. Take out the container, and take out the porous prefabricated body after cooling for later...

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Abstract

The invention discloses a preparation method of a porous preform. The preparation method comprises the following steps of S100, stacking inorganic salt particles in a container with a closed bottom end to form an inorganic salt particle accumulation body; S200, enabling the inorganic salt particle accumulation body to have initial compactness in the container by adopting a compaction method; S300,applying a downward constant pressure of 1-10 MPa to the upper part of the inorganic salt particle accumulation body, heating the container filled with the inorganic salt particle accumulation body to 0.2-0.8 Tm at a heating rate of 5-20 DEG C, and carrying out heat preservation; and S400, keeping the temperature for 1-8 hours, so that the inorganic salt particles creep and deform. The inventionalso discloses a porous preform. The invention further discloses a preparation method of the foam metal. The invention further discloses the foam metal.

Description

technical field [0001] The invention relates to the technical field of metal foam, in particular to a porous preform and a preparation method thereof, as well as metal foam and a preparation method thereof. Background technique [0002] In nature, there are honeycomb structures such as wood and cork, and foam structures such as bones, plant parenchyma, and sponges. These porous structures are light in weight and have excellent mechanical properties, which meet the load-bearing requirements required by organisms. Inspired by these naturally occurring porous materials, people introduce porous structures into metal materials and prepare porous metals to make metal materials meet performance requirements while reducing weight, thereby further expanding the application range of metal materials. The pores in metal foam are functional phases, which not only retain the structural material properties of metal, but also have functional material properties such as energy absorption, sh...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/08
CPCC22C1/08C22C1/082
Inventor 刘源万坦陈祥张华伟
Owner TSINGHUA UNIV
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