Fixed Bed Flow Reactor and Its Application

A reactor and fixed bed technology, which is applied in the field of upflow reactors, can solve problems such as clogging distributors, affecting fluid distribution, clogging, etc., and achieve the effects of alleviating the increase in pressure drop, reducing dust generation, and reducing wear

Active Publication Date: 2021-06-04
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Since the catalyst particles cannot pass through the small bed support gap, these particles are likely to block the distributor or bed support, resulting in uneven distribution of fluid, especially gas, which affects the distribution of fluid in the reactor and affects the reaction process. adversely affect
At the same time, it will also be accompanied by the wear and pulverization of the catalyst particles, resulting in a large amount of catalyst dust. These dusts move upward with the reaction materials, and clogging occurs on the surface of the screen or grid, resulting in a rapid increase in the pressure drop of the bed, affecting response start cycle

Method used

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  • Fixed Bed Flow Reactor and Its Application
  • Fixed Bed Flow Reactor and Its Application
  • Fixed Bed Flow Reactor and Its Application

Examples

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Embodiment 1

[0055] Using the upflow reactor described in the present invention, the raw material oil and hydrogen I are mixed using a conventional static mixer (model SV2.3 / 25-6.4-500), and then the mixture is introduced into the upflow as reactor feed Type reactor (the diameter of the reactor is 100mm), hydrogen II is introduced into the hydrogen inlet of the linkage filter dust layer, wherein the mass ratio of hydrogen I to hydrogen II is 5:1; the direction of material flow in the reactor is as follows: The sliding grille is 100mm, the first catalyst bed is 600mm, the linkage filter dust layer is 260mm, the second catalyst bed is 800mm, the upper sliding grille is 80mm; the lower sliding grille includes slideways and grille plates, and the slideway length is 100mm ;The upper sliding grille includes a slideway and a grille plate, and the length of the slideway is 80mm; the linkage type filter dust layer includes an upper linkage layer, a filter dust layer, and a lower linkage layer; the u...

Embodiment 2

[0057] Using the upflow reactor of the present invention, the raw material oil and hydrogen I are mixed with a conventional static mixer (model SV2.3 / 25-6.4-500), and then the mixture is introduced into the upflow as reactor feed type reactor (the diameter of the reactor is 100mm), the hydrogen gas II is introduced into the hydrogen inlet of the linkage filter dust layer, and the mass ratio of the hydrogen gas I to the hydrogen gas II is 3:1; the flow direction of the material in the reactor is as follows The sliding grille is 100mm, the first catalyst bed layer is 500mm, the linkage filter dust layer is 200mm, the second catalyst bed layer is 600mm, the upper sliding grille is 80mm, and the gland is 100mm; the lower sliding grille includes slideways and grille plates, sliding The length of the channel is 100mm; the upper sliding grille includes the slideway and the grille plate, and the length of the slideway is 80mm; the linkage type filter dust layer includes the upper linka...

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Abstract

The invention discloses a fixed-bed flow reactor and an application thereof. The reactor comprises a reactor shell, in which a lower sliding grid, a first catalyst bed, and a linkage filter unit are arranged along the direction of material flow. Dust layer, second catalyst bed layer, and upper sliding grille; the linked filter dust accumulation layer is fixedly connected to the upper sliding grille and the lower sliding grille respectively through support rods, and the reaction material inlet is set at the bottom of the reactor shell , the top of the reactor shell is equipped with a reaction material outlet; the reactor is equipped with a linkage filter dust layer, which can effectively reduce the movement wear between catalyst particles, improve the service life of the catalyst, and continuously remove catalyst dust during the reaction process , improve the uniformity of the reaction, greatly slow down the rise in the pressure drop of the catalyst bed, and maintain the long-term stable operation of the reactor.

Description

technical field [0001] The invention belongs to the field of petrochemical equipment, and relates to an upflow reactor and its application. Background technique [0002] In the field of petrochemical industry, hydrogenation process is an important technical means for processing distillate oil and secondary processed oil. Through hydrogenation, impurities such as sulfur, nitrogen, metals, colloids, and residual carbon in oil products can be effectively removed. Removal and hydrogenation of unsaturated hydrocarbons to saturated hydrocarbons. According to the type of reactor, the hydrogenation process can be divided into fixed bed hydrogenation process, suspension bed hydrogenation process and ebullated bed hydrogenation process, among which the fixed bed hydrogenation process is the most widely used. [0003] According to the feeding method of the fixed bed reactor, it can be divided into two types: upflow type, that is, bottom feed and downflow type, that is, top feed fixed ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/04C10G49/00
CPCB01J8/0446B01J8/0492B01J2208/00884C10G49/00C10G2300/4006C10G2300/4012
Inventor 周嘉文杨秀娜阮宗琳王昊晨姜阳崔国英关明华
Owner CHINA PETROLEUM & CHEM CORP
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